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Studies of Interface Demarcation and Structural Defects in Ga Doped Ge Single Crystals Using Synchrotron White Beam X-Ray Topography

Published online by Cambridge University Press:  15 February 2011

H. Chung
Affiliation:
Dept. of Materials Science & Engineering, SUNY at Stony Brook, NY 11794–2275.
B. Raghothamachar
Affiliation:
Dept. of Materials Science & Engineering, SUNY at Stony Brook, NY 11794–2275.
W. Zhou
Affiliation:
Dept. of Materials Science & Engineering, SUNY at Stony Brook, NY 11794–2275.
M. Dudley
Affiliation:
Dept. of Materials Science & Engineering, SUNY at Stony Brook, NY 11794–2275.
D. C. Gillies
Affiliation:
NASA, Marshall Space Flight Center, Huntsville, AL 35812.
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Abstract

Synchrotron White Beam X-ray Topography (SWBXT) has been applied to the characterization of marked growth interfaces in Ga doped Ge single crystals. The techniques employed in interface demarcation include modifications of the cold zone temperature, mechanical pulsing and Peltier pulsing. As revealed by our observations, the visibility of growth interfaces is a sensitive function of diffraction conditions. A combination of the correct orientation of the active reciprocal lattice vector with respect to the interface plane and the necessary strain sensitivity controlled by the rocking curve width of the reflection are proved to be important for interface visibility. This can easily be achieved by using synchrotron radiation since the tunability of the synchrotron source provides great flexibility in the choice of proper diffraction conditions. Structural defects such as small-angle tilt boundaries and dislocation cell structures were also observed. The formation mechanism of these defects will be discussed. Direct evidence of dislocations present in the seed crystal propagating into the as-grown crystal through the melt-back interface during crystal growth was also obtained.

Type
Research Article
Copyright
Copyright © Materials Research Society 1996

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References

[1] Chang, C. E. and Wilcox, W. R., J. Cryst. Growth 21, 135 (1974).Google Scholar
[2] Bourret, E. D., Derby, J. J., Brown, R. A. and Witt, A. F., Acta Astronautica 11, 163 (1984).Google Scholar
[3] Huang, Y., Debnam, W. J. and Fripp, A. L., J. Cryst. Growth 104, 315 (1990).Google Scholar
[4] Dudley, M. in Applications of Synchrotron Radiation Techniques to Materials Science, edited by Perry, D.L., Stockbauer, R.L., Shinn, N.D., D'Amico, K.L., and Terminello, L.J., (Mater. Res. Soc. Symp. Proc. 307, Pittsburgh, PA 1993), pp. 213224.Google Scholar
[5] Dudley, M. in, Encyclopedia of Advanced Materials, 4, edited by Bloor, D., Brook, R.J., Flemings, M.C. and Mahajan, S. (Pergamon, 1994), p. 2950.Google Scholar
[6] Gillies, D. C., Lehoczky, S. L., Szofran, F. R., Su, Ching-hua, and Larson, D. J., Proc. of the SPIE 1484, 2 (1991).Google Scholar
[7] Srlnivas, R., Hambright, G., Ainsworth, M., Fiske, M., and Schaefer, D., AIAA 94–0334Google Scholar
[8] Klapper, H. in, Characterization of Crystal Growth Defects by X-ray Methods, edited by Tanner, B. K. and Bowen, D. K. (Plenum, 1980), p. 133.Google Scholar