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X-ray powder diffraction data for [Ru(II) Cl η -6-p-cymene (1R,2R)-N-[((1R,2R)-7,7-dimethyl-2-hydroxy-bicyclo-[2.2.1]- heptan-1-yl)-methansulphonyl]-1,2-diphenylethylene-1,2-diamine] complex

Published online by Cambridge University Press:  23 April 2013

R. Pažout ,
J. Maixner ,
J. Přech  and
P. Kačer
R. Pažout*
Affiliation:
Central Laboratories, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
J. Maixner
Affiliation:
Central Laboratories, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
J. Přech
Affiliation:
Department of Organic Technology, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
P. Kačer
Affiliation:
Department of Organic Technology, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
*
a)Author to whom correspondence should be addressed. Electronic mail: richard.pazout@vscht.cz
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Abstract

X-ray powder diffraction data, unit-cell parameters, and space group for a new Ru Cl diamide complex, C36H48N2SO3RuCl, are reported [a = 12.487(4) Å, b = 16.624(5) Å, c = 17.230(3) Å, unit-cell volume V = 3576,79 Å3, Z = 4, and space group P212121]. All measured lines were indexed and are consistent with the P212121 space group. No detectable impurity was observed.

Keywords

X-ray powder diffractionRu Cl diamide complex
Type
New Diffraction Data
Information
Powder Diffraction , Volume 28 , Issue 3 , September 2013 , pp. 237 - 239
Copyright
Copyright © International Centre for Diffraction Data 2013 

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References

Boultif, A. and Louër, D. (2004). “Powder pattern indexing with the dichotomy method,” J. Appl. Crystallogr. 37, 724–731.CrossRefGoogle Scholar
De Wolff, P. M. (1968). “A simplified criterion for the reliability of a powder pattern indexing,” J. Appl. Crystallogr. 1, 108–113.CrossRefGoogle Scholar
Smith, G. S. and Snyder, R. L. (1979). “FN: a criterion for rating powder diffraction patterns and evaluating the reliability of powder indexing,” J. Appl. Crystallogr. 12, 60–65.CrossRefGoogle Scholar
Uematsu, N., Fujii, A., Hashiguchi, S., Ikariya, T., and Noyori, R. (1996). “Asymmetric transfer hydrogenation of imines,” J. Am. Chem. Soc. 118, 4916–4917.CrossRefGoogle Scholar