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Formation of BaPbO3-x and BaPb1/3Bi2/3O3-x from Ba(COO)2⋅0.5H2O and Pb(COO)2 oxalates

Published online by Cambridge University Press:  29 July 2020

Barys Korzun ,
Alena Fadzeyeva  and
Joel Hernandez
Barys Korzun
Affiliation:
The City University of New York, Borough of Manhattan Community College, 199 Chambers St., New York, NY10007, U.S.A.
Alena Fadzeyeva
Affiliation:
Scientific-Practical Materials Research Centre of the National Academy of Sciences of Belarus, 19 P. Brovki, Minsk220072, Belarus
Joel Hernandez
Affiliation:
The City University of New York, Borough of Manhattan Community College, 199 Chambers St., New York, NY10007, U.S.A.
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Abstract

This paper reports a way to obtain BaPbO3-x and BaPb1/3Bi2/3O3-x perovskite-type compounds. The method is based on the initial preparation of Ba(COO)2⋅0.5H2O and Pb(COO)2⋅oxalates, and the subsequent calcination of the equimolar physical mixture of these oxalates until the desired compounds BaPbO3-x and BaPb1/3Bi2/3O3-x are formed. To obtain BaPb1/3Bi2/3O3-x, the oxide Bi2O3 is added to the mixture of oxalates and calcined together with them. The temperature for the formation of BaPbO3-x and BaPb1/3Bi2/3O3-x was estimated to be 850°C. These final compounds prepared by calcination were composed of a single phase and exhibited monoclinic crystal structure. The thermal decomposition of the Pb(COO)2 oxalate and the formation of BaPbO3-x and BaPb1/3Bi2/3O3-x were investigated by X-ray powder diffraction (XRPD) and differential thermal analysis (DTA).

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Articles
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MRS Advances , Volume 5 , Issue 51: Characterization and Theory , 2020 , pp. 2647 - 2658
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Copyright
Copyright © Materials Research Society 2020

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