Skip to main content Accessibility help
×
Hostname: page-component-7479d7b7d-68ccn Total loading time: 0 Render date: 2024-07-13T16:23:19.819Z Has data issue: false hasContentIssue false

5 - Low-temperature scanning electron microscopy

Published online by Cambridge University Press:  21 August 2009

Nigel D. Browning
Affiliation:
University of Illinois, Chicago
Stephen J. Pennycook
Affiliation:
Oak Ridge National Laboratory, Tennessee
Get access

Summary

Introduction

Scanning techniques for obtaining topographical information about an object are now widely used in science and technology. Usually, a two-dimensional image is constructed from the signal generated by the scanning process, and this information is restricted to a region close to the sample surface. [5.1]. Here a well focused electron beam is scanned over the surface of the specimen and a response signal such as the emitted secondary electrons or the back-scattered electrons are recorded as a function of the coordinate point (x, y) of the beam focus on the sample surface. We emphasize that this technique essentially yields only information about the composition (atomic, chemical, or metallurgical microstructure) and the geometry of the specimen.

Some time ago, low-temperature scanning electron microscopy (LTSEM) was introduced [5.2] which by now has matured into an important new diagnostic tool. LTSEM extends the temperature of scanning electron microscopy to the regime of liquid helium and liquid nitrogen by providing the necessary sample cooling. However, more importantly, LTSEM yields information on the local electronic function and not just the local structure with high spatial resolution. In this way it has provided important input for the understanding of the physics of superconducting electronic circuits and devices. Of course, LTSEM is equally important for the evaluation and analysis of low Tc and high Tc superconductors. The principle of LTSEM utilizes the electron beam as a local heat source on the one hand, and the sensitive response of superconductors to small temperature changes on the other hand [5.2].

Type
Chapter
Information
Publisher: Cambridge University Press
Print publication year: 2000

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

Save book to Kindle

To save this book to your Kindle, first ensure coreplatform@cambridge.org is added to your Approved Personal Document E-mail List under your Personal Document Settings on the Manage Your Content and Devices page of your Amazon account. Then enter the ‘name’ part of your Kindle email address below. Find out more about saving to your Kindle.

Note you can select to save to either the @free.kindle.com or @kindle.com variations. ‘@free.kindle.com’ emails are free but can only be saved to your device when it is connected to wi-fi. ‘@kindle.com’ emails can be delivered even when you are not connected to wi-fi, but note that service fees apply.

Find out more about the Kindle Personal Document Service.

Available formats
×

Save book to Dropbox

To save content items to your account, please confirm that you agree to abide by our usage policies. If this is the first time you use this feature, you will be asked to authorise Cambridge Core to connect with your account. Find out more about saving content to Dropbox.

Available formats
×

Save book to Google Drive

To save content items to your account, please confirm that you agree to abide by our usage policies. If this is the first time you use this feature, you will be asked to authorise Cambridge Core to connect with your account. Find out more about saving content to Google Drive.

Available formats
×