Hostname: page-component-8448b6f56d-gtxcr Total loading time: 0 Render date: 2024-04-19T14:26:19.097Z Has data issue: false hasContentIssue false

Effect of ceramic particle size on densification behavior, microstructure formation, and performance of TiB2-reinforced Al-based composites prepared by selective laser melting

Published online by Cambridge University Press:  17 January 2020

Lixia Xi
Affiliation:
College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China; and Jiangsu Provincial Engineering Laboratory for Laser Additive Manufacturing of High-Performance Metallic Components, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China
Dongdong Gu*
Affiliation:
College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China; and Jiangsu Provincial Engineering Laboratory for Laser Additive Manufacturing of High-Performance Metallic Components, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China
Kaijie Lin
Affiliation:
College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China; and Jiangsu Provincial Engineering Laboratory for Laser Additive Manufacturing of High-Performance Metallic Components, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China
Shuang Guo
Affiliation:
College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China; and Jiangsu Provincial Engineering Laboratory for Laser Additive Manufacturing of High-Performance Metallic Components, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China
Yang Liu
Affiliation:
College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China; and Jiangsu Provincial Engineering Laboratory for Laser Additive Manufacturing of High-Performance Metallic Components, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China
Yuxin Li
Affiliation:
College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China; and Jiangsu Provincial Engineering Laboratory for Laser Additive Manufacturing of High-Performance Metallic Components, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China
Meng Guo
Affiliation:
College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China; and Jiangsu Provincial Engineering Laboratory for Laser Additive Manufacturing of High-Performance Metallic Components, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China
*
a)Address all correspondence to this author. e-mail: dongdonggu@nuaa.edu.cn
Get access

Abstract

Al-based composites with micrometer and submicro-TiB2 reinforcements (1 wt%) have been produced by selective laser melting (SLM) from mixed powder under different processing conditions. The results show that the densification level of SLM-processed composite with submicro-TiB2 particles (>99.0%) was 0.3–2.4% larger than that of micrometer TiB2-reinforced composite under the same processing conditions. The distribution of Si precipitates in the matrix experienced a transform from continuous cellular to directional line-like morphology with reinforcement size decreasing from micron to submicron. The reinforcement size added in the matrix also exhibited a critical influence on preferred orientation and grain size of matrix. The SLM-processed composites exhibited improved tensile strength and ductility with a decrease of reinforcement size. High tensile strength of 400 MPa and elongation of 3.6% were obtained for the fine TiB2-reinforced samples, increasing by 6 and 13% compared with that of micro-TiB2–added samples, respectively.

Type
Article
Copyright
Copyright © Materials Research Society 2020

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Herzog, D., Seyda, V., Wycisk, E., and Emmelmann, C.: Additive manufacturing of metals. Acta Mater. 117, 371 (2016).CrossRefGoogle Scholar
Gu, D.: Laser Additive Manufacturing of High-Performance Materials (Springer, Berlin, London, 2015).CrossRefGoogle Scholar
Collins, P.C., Brice, D.A., Samimi, P., Ghamarian, I., and Fraser, H.L.: Microstructural control of additively manufactured metallic materials. Annu. Rev. Mater. Res. 46, 63 (2016).CrossRefGoogle Scholar
Zhang, L.C., Klemm, D., Eckert, J., Hao, Y.L., and Sercombe, T.B.: Manufacture by selective laser melting and mechanical behavior of a biomedical Ti–24Nb–4Zr–8Sn alloy. Scr Mater 65, 21 (2011).CrossRefGoogle Scholar
AlMangour, B., Grzesiak, D., and Jenn, M.: Selective laser melting of TiC reinforced 316L stainless steel matrix nanocomposites: Influence of starting TiC particle size and volume content. Mater. Des. 104, 141 (2016).CrossRefGoogle Scholar
Liu, Y.J., Li, S.J., Wang, H.L., Hou, W.T., Hao, Y.L., Yang, R., Sercombe, T.B., and Zhang, L.C.: Microstructure, defects and mechanical behavior of beta-type titanium porous structures manufactured by electron beam melting and selective laser melting. Acta Mater. 113, 56 (2016).CrossRefGoogle Scholar
Gu, D., Wang, H., Dai, D., Yuan, P., Meiners, W., and Poprawe, R.: Rapid fabrication of Al-based bulk-form nanocomposites with novel reinforcement and enhanced performance by selective laser melting. Scr Mater 96, 25 (2015).CrossRefGoogle Scholar
Yadroitsev, I. and Smurov, I.: Selective laser melting technology: From the single laser melted track stability to 3D parts of complex shape. Phys. Procedia 5, 551 (2010).CrossRefGoogle Scholar
AlMangour, B., Grzesiak, D., and Yang, J-M.: In situ formation of TiC-particle-reinforced stainless steel matrix nanocomposites during ball milling: Feedstock powder preparation for selective laser melting at various energy densities. Powder Technol. 326, 467 (2018).CrossRefGoogle Scholar
Li, X., Kong, C., Becker, T., and Sercombe, T.: Investigation of interfacial reaction products and stress distribution in selective laser melted Al12Si/SiC composite using confocal Raman microscopy. Adv. Eng. Mater. 18, 1337 (2016).CrossRefGoogle Scholar
Gu, D., Shen, Y., and Meng, G.: Growth morphologies and mechanisms of TiC grains during selective laser melting of Ti–Al–C composite powder. Mater. Lett. 63, 2536 (2009).CrossRefGoogle Scholar
Tjong, S.C. and Ma, Z.Y.: Microstructural and mechanical characteristics of in situ metal matrix composites. Mater. Sci. Eng., R 29, 49 (2000).CrossRefGoogle Scholar
Li, X.P., Ji, G., Chen, Z., Addad, A., Wu, Y., Wang, H.W., Vleugels, J., Van Humbeeck, J., and Kruth, J.P.: Selective laser melting of nano-TiB2 decorated AlSi10Mg alloy with high fracture strength and ductility. Acta Mater. 129, 183 (2017).CrossRefGoogle Scholar
Gu, D.D., Meiners, W., Wissenbach, K., and Poprawe, R.: Laser additive manufacturing of metallic components: Materials, processes and mechanisms. Int. Mater. Rev. 57, 133 (2012).CrossRefGoogle Scholar
Gu, D. and Meiners, W.: Microstructure characteristics and formation mechanisms of in situ WC cemented carbide based hardmetals prepared by selective laser melting. Mater. Sci. Eng., A 527, 7585 (2010).CrossRefGoogle Scholar
Dadbakhsh, S., Mertens, R., Hao, L., Van Humbeeck, J., and Kruth, J.P.: Selective laser melting to manufacture “in situ” metal matrix composites: A review. Adv. Eng. Mater. 21, 1801244 (2019).CrossRefGoogle Scholar
Chang, F., Gu, D., Dai, D., and Yuan, P.: Selective laser melting of in situ Al4SiC4 + SiC hybrid reinforced Al matrix composites: Influence of starting SiC particle size. Surf. Coat. Technol. 272, 15 (2015).CrossRefGoogle Scholar
Xi, L., Wang, P., Prashanth, K.G., Li, H., Prykhodko, H.V., Scudino, S., and Kaban, I.: Effect of TiB2 particles on microstructure and crystallographic texture of Al–12Si fabricated by selective laser melting. J. Alloys Compd. 786, 551 (2019).CrossRefGoogle Scholar
Yadav, S., Aggrawal, A., Kumar, A., and Biswas, K.: Effect of TiB2 addition on wear behavior of (AlCrFeMnV)90Bi10 high entropy alloy composite. Tribol. Int. 132, 62 (2019).CrossRefGoogle Scholar
Xi, L., Kaban, I., Nowak, R., Korpała, B., Bruzda, G., Sobczak, N., Mattern, N., and Eckert, J.: High-temperature wetting and interfacial interaction between liquid Al and TiB2 ceramic. J. Mater. Sci. 50, 2682 (2015).CrossRefGoogle Scholar
Xiao, Y.K., Bian, Z.Y., Wu, Y., Ji, G., Li, Y.Q., Li, M.J., Lian, Q., Chen, Z., Addad, A., and Wang, H.W.: Effect of nano-TiB2 particles on the anisotropy in an AlSi10Mg alloy processed by selective laser melting. J. Alloys Compd. 798, 644 (2019).CrossRefGoogle Scholar
Xi, L.X., Zhang, H., Wang, P., Li, H.C., Prashanth, K.G., Lin, K.J., Kaban, I., and Gu, D.D.: Comparative investigation of microstructure, mechanical properties and strengthening mechanisms of Al–12Si/TiB2 fabricated by selective laser melting and hot pressing. Ceram. Int. 44, 17635 (2018).CrossRefGoogle Scholar
Xi, L., Guo, S., Gu, D., Guo, M., and Lin, K.: Microstructure development, tribological property and underlying mechanism of laser additive manufactured submicro-TiB2 reinforced Al-based composites. J. Alloys Compd. 80, 152980 (2019).Google Scholar
Lai, S.L., Guo, J.Y., Petrova, V., Ramanath, G., and Allen, L.H.: Size-dependent melting properties of small tin particles: Nanocalorimetric measurements. Phys. Rev. Lett. 77, 99 (1996).CrossRefGoogle ScholarPubMed
Lampa, C.A., Kaplan, A., Resch, M., and Magnusson, C.: Fluid flow and resolidification in deep penetration laser welding. Lasers Eng. 7, 241 (1998).Google Scholar
Gu, D. and Shen, Y.: Effects of processing parameters on consolidation and microstructure of W–Cu components by DMLS. J. Alloys Compd. 473, 107 (2009).CrossRefGoogle Scholar
Prashanth, K.G., Scudino, S., Klauss, H.J., Surreddi, K.B., Löber, L., Wang, Z., Chaubey, A.K., Kühn, U., and Eckert, J.: Microstructure and mechanical properties of Al–12Si produced by selective laser melting: Effect of heat treatment. Mater. Sci. Eng., A 590, 153 (2014).CrossRefGoogle Scholar
Zhao, X., Song, B., Fan, W., Zhang, Y., and Shi, Y.: Selective laser melting of carbon/AlSi10Mg composites: Microstructure, mechanical and electronical properties. J. Alloys Compd. 665, 271 (2016).CrossRefGoogle Scholar
Wang, Z., Prashanth, K.G., Chaubey, A.K., Löber, L., Schimansky, F.P., Pyczak, F., Zhang, W.W., Scudino, S., and Eckert, J.: Tensile properties of Al–12Si matrix composites reinforced with Ti–Al-based particles. J. Alloys Compd. 630, 256 (2015).CrossRefGoogle Scholar
Chen, B., Moon, S.K., Yao, X., Bi, G., Shen, J., Umeda, J., and Kondoh, K.: Strength and strain hardening of a selective laser melted AlSi10Mg alloy. Scr Mater 141, 45 (2017).CrossRefGoogle Scholar
Li, X.P., Wang, X.J., Saunders, M., Suvorova, A., Zhang, L.C., Liu, Y.J., Fang, M.H., Huang, Z.H., and Sercombe, T.B.: A selective laser melting and solution heat treatment refined Al–12Si alloy with a controllable ultrafine eutectic microstructure and 25% tensile ductility. Acta Mater. 95, 74 (2015).CrossRefGoogle Scholar
AlMangour, B., Grzesiak, D., and Yang, J-M.: Selective laser melting of TiB2/316L stainless steel composites: The roles of powder preparation and hot isostatic pressing post-treatment. Powder Technol. 309, 37 (2017).CrossRefGoogle Scholar
Li, Y. and Gu, D.: Parametric analysis of thermal behavior during selective laser melting additive manufacturing of aluminum alloy powder. Mater. Des. 63, 856 (2014).CrossRefGoogle Scholar
Pinkerton, A.J. and Li, L.: The effect of laser pulse width on multiple-layer 316L steel clad microstructure and surface finish. Appl. Surf. Sci. 208–209, 411 (2003).CrossRefGoogle Scholar
Wei, P., Wei, Z., Chen, Z., Du, J., He, Y., Li, J., and Zhou, Y.: The AlSi10Mg samples produced by selective laser melting: Single track, densification, microstructure and mechanical behavior. Appl. Surf. Sci. 408, 38 (2017).CrossRefGoogle Scholar
Delroisse, P., Jacques, P.J., Maire, E., Rigo, O., and Simar, A.: Effect of strut orientation on the microstructure heterogeneities in AlSi10Mg lattices processed by selective laser melting. Scr. Mater. 141, 32 (2017).CrossRefGoogle Scholar
Espana, F.A., Balla, V.K., and Bandyopadhyay, A.: Laser processing of bulk Al–12Si alloy: Influence of microstructure on thermal properties. Philos. Mag. 91, 574 (2011).CrossRefGoogle Scholar
Zhang, S., Ma, P., Jia, Y., Yu, Z., Sokkalingam, R., Shi, X., Ji, P., Eckert, J., and Prashanth, K.G.: Microstructure and mechanical properties of Al–(12-20)Si bi-material fabricated by selective laser melting. Materials 12, 2126 (2019).CrossRefGoogle ScholarPubMed
AlMangour, B., Grzesiak, D., and Yang, J-M.: Rapid fabrication of bulk-form TiB2/316L stainless steel nanocomposites with novel reinforcement architecture and improved performance by selective laser melting. J. Alloys Compd. 680, 480 (2016).CrossRefGoogle Scholar
Dai, D. and Gu, D.: Tailoring surface quality through mass and momentum transfer modeling using a volume of fluid method in selective laser melting of TiC/AlSi10Mg powder. Int. J. Mach. Tool Manuf. 88, 95 (2015).CrossRefGoogle Scholar
Dai, D. and Gu, D.: Influence of thermodynamics within molten pool on migration and distribution state of reinforcement during selective laser melting of AlN/AlSi10Mg composites. Int. J. Mach. Tool Manuf. 100, 14 (2016).CrossRefGoogle Scholar
Zhang, B., Bi, G., Nai, S., Sun, C-n., and Wei, J.: Microhardness and microstructure evolution of TiB2 reinforced Inconel 625/TiB2 composite produced by selective laser melting. Opt. Laser Technol. 80, 186 (2016).CrossRefGoogle Scholar
McCartney, D.G.: Grain refining of aluminium and its alloys using inoculants. Int. Mater. Rev. 34, 247 (1989).CrossRefGoogle Scholar
Murty, B.S., Kori, S.A., and Chakraborty, M.: Grain refinement of aluminium and its alloys by heterogeneous nucleation and alloying. Int. Mater. Rev. 47, 3 (2002).CrossRefGoogle Scholar
Fan, Z., Wang, Y., Zhang, Y., Qin, T., Zhou, X.R., Thompson, G.E., Pennycook, T., and Hashimoto, T.: Grain refining mechanism in the Al/Al–Ti–B system. Acta Mater. 84, 292 (2015).CrossRefGoogle Scholar
Jiang, W.H. and Kovacevic, R.: Laser deposited TiC/H13 tool steel composite coatings and their erosion resistance. J. Mater. Process. Technol. 186, 331 (2007).CrossRefGoogle Scholar
Yang, Y., Gu, D., Dai, D., and Ma, C.: Laser energy absorption behavior of powder particles using ray tracing method during selective laser melting additive manufacturing of aluminum alloy. Mater. Des. 143, 12 (2018).CrossRefGoogle Scholar
Loh, L-E., Chua, C-K., Yeong, W-Y., Song, J., Mapar, M., Sing, S-L., Liu, Z-H., and Zhang, D-Q.: Numerical investigation and an effective modelling on the selective laser melting (SLM) process with aluminium alloy 6061. Int. J. Heat Mass Transfer 80, 288 (2015).CrossRefGoogle Scholar
Dai, D., Gu, D., Poprawe, R., and Xia, M.: Influence of additive multilayer feature on thermodynamics, stress and microstructure development during laser 3D printing of aluminum-based material. Sci. Bull. 62, 779 (2017).CrossRefGoogle Scholar
Read, N., Wang, W., Essa, K., and Attallah, M.M.: Selective laser melting of AlSi10Mg alloy: Process optimisation and mechanical properties development. Mater. Des. 65, 417 (2015).CrossRefGoogle Scholar
AlMangour, B., Grzesiak, D., Borkar, T., and Yang, J-M.: Densification behavior, microstructural evolution, and mechanical properties of TiC/316L stainless steel nanocomposites fabricated by selective laser melting. Mater. Des. 138, 119 (2018).CrossRefGoogle Scholar
Lu, K.: The future of metals. Science 328, 319 (2010).CrossRefGoogle ScholarPubMed
Tjong, S.C.: Novel nanoparticle-reinforced metal matrix composites with enhanced mechanical properties. Adv. Eng. Mater. 9, 639 (2007).CrossRefGoogle Scholar