Dating ice samples from glaciers via radiocarbon is a challenge that requires systematic investigations. This work describes an approach for extraction and accelerator mass spectrometry (AMS) 14C analysis of the particulate organic carbon (POC) fraction in glacier ice samples. Measurements were performed at VERA (Vienna Environmental Research Accelerator) on ice samples obtained mainly from the non-temperated ablation zone of the Grenzgletscher (Grenz Glacier) system (Monte Rosa Massif, Swiss Alps). The samples were obtained from 2 sampling sites situated roughly on a common flow line. The sample masses used were between 0.3 and 1.4 kg of ice, yielding between 18 and 307 μg of carbon as POC. The carbon contamination introduced during sample processing varied between 5.4 and 33 μg C and originated mainly from the quartz filters and the rinsing liquids used in processing. Minimum sample sizes for successful graphitization of CO2 in our laboratory could be reduced to <10 μg carbon, with a background in the graphitization process of ∼0.5 μg of 40-pMC carbon. Evaluation of the whole procedure via 11 Grenzgletscher samples revealed a surprisingly large scatter of pMC values. We obtain a mean calibrated age of 2100 BC to AD 900 (95.4% confidence level), which is not significantly different for the 2 sampling sites. Discussions of these results suggest that single 14C dates of glacial POC are presently of limited significance. Future improvements with respect to analytical precision and sample characterization are proposed in order to fully explore the POC dating potential.

A chronological synthesis of prehistoric campsites in alpine and subalpine zones (∼2–3 km asl) at Haleakalā, Maui Island, USA, is based on relative stratigraphy from 24 test excavations, associated artifacts of known or probable time periods, and 12 radiocarbon dates. The results indicate intensive use of the unfavorable high-altitude environment in the range of AD 1400–1600, with very limited use slightly earlier. Numerous campsites were used repeatedly near the Haleakalā crater rim and scattered on the lower western mountain slope. Prior to this time, activity in this inhospitable setting was infrequent and occurred on a small scale.

A recently published volume, The Bible and Radiocarbon Dating: Archaeology, Text and Science (Levy and Higham 2005), provides data related to the debate over the chronology of the Iron Age strata in the Levant (for a review, see Carmi 2006). The present article comments on several chapters in the volume. The article highlights methodological problems, such as insecure stratigraphic provenance of 14C samples, and demonstrates how unjustified selection of data can bias the result. The article offers a new interpretation to some of the results and shows that the full set of measurements from Tel Rehov supports the Low Chronology system.

Archaeometry is becoming an increasingly important tool in chronological research related to events in the Ancient Near East during the 2nd millennium BCE. This paper is a review of recently published radiometric results in an attempt to establish the probable dating range for one particular event that occurred during the last quarter of that millennium, the end of the Late Bronze Age. The conclusion is that in spite of significant improvements in methodology in recent years, the quantity and quality of radiocarbon data are still insufficient to define the range of that date to much better than a century. It is concluded that the most likely date of the Late Bronze/Iron Age transition (here defined by the arrival of Mycenaean LH IIIC:1b pottery in the Levant) is somewhere in the 8-decade range between ∼1170 to 1100 BCE. A comparative study of archaeological and historical evidence would appear to favor the lower value.

We demonstrate variable radiocarbon content within 2 historic (AD 1936) and 2 prehistoric (about 8200 BP and 3500 BP) Mytilus californianus shells from the Santa Barbara Channel region, California, USA. Historic specimens from the mainland coast exhibit a greater range of intrashell variability (i.e. 180–240 14C yr) than archaeological specimens from Daisy Cave on San Miguel Island (i.e. 120 14C yr in both shells). δ13C and δ18O profiles are in general agreement with the up welling of deep ocean water depleted in 14C as a determinant of local marine reservoir correction (ΔR) in the San Miguel Island samples. Upwelling cycles are difficult to identify in the mainland specimens, where intrashell variations in 14C content may be a complex product of oceanic mixing and periodic seasonal inputs of 14C-depeleted terrestrial runoff. Though the mechanisms controlling ΔR at subannual to annual scales are not entirely clear, the fluctuations represent significant sources of random dating error in marine environments, particularly if a small section of shell is selected for accelerator mass spectrometry (AMS) dating. For maximum precision and accuracy in AMS dating of marine shells, we recommend that archaeologists, paleontologists, and 14C lab personnel average out these variations by sampling across multiple increments of growth.

In the journal Radiocarbon, Hall et al. (2005:383) claim that 35-CS-9, located in Bandon Ocean Wayside State Park on the southern Oregon coast, is one of the few Oregon coast sites “that includes sediments and artifacts dating to the early Holocene and possibly to the late Pleistocene.” Their claim for an early Holocene or late Pleistocene human occupation rests on a single radiocarbon date of 11,000 ± 140 BP (12,710–12,680 cal BP) taken from charcoal found at least 20 cm below the nearest artifact. Although Hall et al. compile various kinds of geoarchaeological evidence to support this claim, their case is not convincing. While we applaud aspects of their analyses, the inferences they have drawn are not substantiated by the evidence they present. We agree that 35-CS-9 is a significant site but believe claims for the antiquity of its human use have been exaggerated.

Several articles reporting radiocarbon dates of Early Bronze Age (EB) material from excavations in the southern Levant have been published over the last 30 yr. The excavations conducted at Tell el-Hesi have produced material from which 2 additional 14C dates have been extracted to date. The 2 samples confirm the EB dating of Field VI material and suggest EB III settlement at Hesi might be earlier than previously reported based on pottery typology.

Radiocarbon ages of 8 decadal tree rings and 66 single-yr tree rings have been measured with a highly accurate liquid scintillation counting (LSC) system (0.2% error) after synthesizing 10.5 g of benzene for each α-cellulose sample produced from tree rings of Choukai Jindai cedar in Japan (39°N). The 14C ages were between 2449 and 2539 14C yr BP for the 21 samples. From the wiggle-matching of the data set using the IntCal04 (Reimer et al. 2004) calibration data in OxCal v 3.10 (Bronk Ramsey 2005), the estimated age of the outer edge of the Choukai tree rings was 477.5 BC (±12.5 yr) with a confidence level of 95.5%; hence, the Choukai tree rings range from 2757 to 2437 cal BP. The age indicates an improved eruption date of the Choukai Volcano. The statistical errors at 1 σ are approximately ± 10 and ± 7 14C yr for the 5-yr data and the decadal data from the single-yr measurements, respectively. For the interval between 2580 and 2520 cal BP, it is statistically significant that the Choukai 14C ages are ∼16 14C yr older on average than both the IntCal04 and QL German oak (∼50°N) data sets. The ∼2.0% offset is informative for the study of regional offset in the Far East.

Accurate and reliable dating of paleosols, animal remains, and artifacts is of crucial importance in reconstructing environmental change and understanding the interrelationship between human activities and natural environments. Dating different materials in the same sample can help resolve problems such as soil carbon sources and carbon storage state. Conventional radiocarbon dating of soil (inorganic and organic matter) and accelerator mass spectrometry (AMS) dating of animal remains (fossil bones and teeth) result in different ages for materials from the same sample position in a typical loess section at Xinglong Mountain, Yuzhong County, Gansu Province in NW China. Inorganic matter is ∼3400 yr older than organic matter, 4175 ± 175 cal BP to 3808 ± 90 cal BP. A 1610-yr difference between the 14C ages of fossils (animal bones and teeth) and soil organic matter suggests that a depositional hiatus exists in the studied profile. The varying 14C ages of fossils and soil organic and inorganic matter have important implications for paleoclimate reconstructions from loess sections. It is critical to consider the meaning of the variable 14C ages from different material components from the same sample position in terms of soil organic and inorganic carbon storage, vegetation history reconstruction, archaeology, and the study of ancient civilizations.

Higham et al.'s (2005) recent article in Radiocarbon 47(3) concerning diet-induced anomalies on radiocarbon ages for various faunal samples from Shag River Mouth is a well-considered study, building upon methodologies and research questions examining the phenomena of dietary anomalies addressed by Beavan Athfield and coauthors (cf. Beavan-Athfield et al. 1999, 2001a; Beavan-Athfield and Sparks 2001a,b,c). However, exception must be taken with one comment appearing in Higham et al. (2005) that suggests to the reader that there is a problem with the laboratory practice associated with rat bone dates measured at the Rafter Radiocarbon Laboratory of GNS Science, New Zealand.

Radiocarbon dates on samples aimed to date the settlement of Iceland are given together with comments by the laboratory, since many of the results and descriptions given by Sveinbjörnsdóttir et al. (2004) in Radiocarbon, together with new results, are in error. The intention of this paper is to present correct dates and further relevant information regarding samples used earlier and to discuss possible complications inherent in the method of Sveinbjörnsdóttir et al. (2004). Examples are given of how critical the collection, treatment, and interpretation of samples may be. An age difference between birch charcoal and grains for a site is expected due to various reasons. If the difference amounts up to ∼100 yr, as reported by Sveinbjörnsdóttir et al. (2004), it must only to a small degree be due to biological age. Reference to an excavation report, details regarding stratigraphy, and discussions of the risk for displacement and contamination are missing in their paper. A final evaluation of the time for settlement should not be done until more research is completed and other possible or earlier suggested or even dated sites are discussed. A summary is given of the research on the island and volcanic effects on the 14C activity of the atmospheric CO2, especially over Iceland.

The chronology of residential site construction and occupation in the upper reaches of the ‘Opunohu Valley, Mo'orea, Central Eastern Polynesia, has been debated over the last 15 yr. This paper reports a suite of 11 radiocarbon age determinations from excavations at 5 house sites and a simple temple structure (marae). Direct accelerator mass spectrometry (AMS) dating of wood charcoal identified to short-lived taxa confirms site construction and occupation during the mid-15th to 17th centuries, supporting that maximal population density was in the centuries immediately prior to European contact. The study demonstrates that targeted dating of multiple structures within residential complexes allows for multiple phases of site construction and use to be discriminated. These data are critical for adequately assessing site contemporaneity and the development, maintenance, and expansion of residential groups and their house clusters through time.

The Balearic Islands are one of the most widely dated regions in Europe, totaling about 800 dates. The aim of this paper is to propose an updated periodization for the prehistory of Majorca and Minorca based on the analysis of a series of absolute dates for over 100 archaeological sites and in combination with a critical assessment of the associated contextual information. Only by means of a solid chronological scheme will we then be able to approach research into the social significance of the vast archaeological record that the islands has to offer and also make reliable comparisons with developments in surrounding regions.

Extensive radiocarbon dating of human remains from Neolithic and Bronze Age hunter-gatherer cemeteries in the Cis-Baikal region of Siberia has been undertaken as a part of the multidisciplinary examination of this material conducted by the Baikal Archaeology Project (BAP; http://baikal.arts.ualberta.ca). Due to the large number of analyzed samples, this paper reports the 14C results only in the context of the basic archaeological information about each of the cemeteries. Comprehensive evaluation, analysis, and interpretation of this entire data set will be undertaken in separate publications. In fact, the dates for one such cemetery have already been examined on 2 recent occasions (Weber et al. 2004, 2005).

The accelerator mass spectrometry facility at Seoul National University (SNU-AMS) began functioning in December 1998 and was first reported at the Vienna AMS conference in October 1999 and at the 17th International Radiocarbon Conference in Israel in June 2000. At the Vienna conference, we reported our accelerator system (Kim et al. 2000) and details of the basic sample preparation system (Lee et al. 2000), such as the combustion line to produce CO2; the catalytic reduction line for the graphitization of CO2; and the pretreatment procedures for wood, charcoal, and peat samples. The recent progress of the AMS facility (Kim et al. 2001) and the extension of the sample pretreatment system to iron and bone samples were reported at the 17th International Radiocarbon Conference (Cheoun et al. 2001). In the meantime, extensive testing of accuracy and reproducibility has been carried out, and ∼1000 unknown archaeological and geological samples have been measured every year. In this report, the archaeological, geological, and environmental data carried out in 1999 are presented in terms of yr BP.

We present results of radiocarbon dating of charcoal from paleosols and buried charcoal horizons in a unique sequence, which potentially records the last 36,000 yr, from a fan at Bear Flat, British Columbia (BC) (56°16'51’N, 121°13'39”W). Evidence for forest-fire charcoal is found over the last 13,500 ± 110 14C yr before present (BP) or 16,250 ± 700 cal BP. The study area is located east of the Rocky Mountains in an area that was ice-free at least 13,970 ± 170 14C yr BP (17,450–16,150 cal BP) ago. The latest evidence of fire is during the Medieval Warm Period (MWP). The charcoal ages show a periodicity in large fires on a millennial scale through the Holocene—an average of 4 fires per thousand years. Higher fire frequencies are observed between 2200 to 2800 cal BP, ∼5500 and ∼6000 cal BP, ∼7500 to 8200 cal BP, and 9000 to 10,000 cal BP. These intervals also appear to be times of above-average aggradation of the fan. We conclude that fire frequency is related to large-scale climatic events on a millennial time scale.

This paper estimates the radioactive graphite dispersion on the land surface (forest litter and soil) as a result of the Chernobyl Nuclear Power Plant (NPP) release. Graphite mass was calculated using an estimated average concentration of 2.5 × 107 Bq/kgC (carbon). The sample collection method, sample origin and its mass, and sample preparation procedure used for preparation of benzene were taken into account to obtain the optimum sensitivity of the method. Thus, the sensitivity of the corresponding method for graphite detection in forest litter was estimated to be 0.2 mg/m2. All analyses gave a range of deposited graphite from 0.12 to 52.6 mg/m2. The maximum value was observed at a site located 9 km west of the Chernobyl NPP. The results of the study indicate the importance of studying the upper layer of soil (0–5 cm) in addition to the lower layer of forest litter.