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X-ray diffraction data of C16H14O4Ru2M (M=Ge,Si)

Published online by Cambridge University Press:  05 March 2012

Yu PuLan ,
Ding Shuang ,
Qiao YuanYuan ,
Yao XinKan ,
Liu Chong  and
Lin ShaoFan
Yu PuLan
Affiliation:
Central Laboratory, Nankai University, Tianjin, China, 300071
Ding Shuang
Affiliation:
Central Laboratory, Nankai University, Tianjin, China, 300071
Qiao YuanYuan
Affiliation:
Central Laboratory, Nankai University, Tianjin, China, 300071
Yao XinKan
Affiliation:
Central Laboratory, Nankai University, Tianjin, China, 300071
Liu Chong
Affiliation:
Central Laboratory, Nankai University, Tianjin, China, 300071
Lin ShaoFan
Affiliation:
Central Laboratory, Nankai University, Tianjin, China, 300071
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Abstract

Two compounds have been studied by means of powder diffraction and their unit cell parameters are reported. The monoclinic cell parameters for dimethylgermanyl-bridged bis cyclopentadienyl tetracarbonyl diruthenium are a=11.03(2) Å, b=13.65(2) Å, c=11.609(2) Å, β=105.81(1)°, Z=4, space group P21/n (No. 14), Dx=2.135 mg/m3. The monoclinic cell parameters for λ-dimethylsilyl-dicyclopentadienyl-π, π′-tetracarbonyl diruthenium, are a=11.113(3) Å, b=13.60(1) Å, c=11.674(7) Å, and β=106.00(3)°, Z=4, space group P21/n (No. 14), and Dx=1.946 mg/m3. The cells found for the two compounds are in good agreement with those obtained from single crystal X-ray diffractometry.

Keywords

Powder dataruthenium
Type
New Diffraction Data
Information
Powder Diffraction , Volume 17 , Issue 1 , March 2002 , pp. 44 - 47
Copyright
Copyright © Cambridge University Press 2002

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References

Xinkan, Yao, Proceedings of Seventh National Conference on X-ray Diffraction (People’s Republic of China, 1997), Vol. 17.Google Scholar