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Powder X-ray diffraction data of a new calcium zirconium phosphate Ca7Zr(PO4)6

Published online by Cambridge University Press:  05 March 2012

Koichiro Fukuda
Affiliation:
Department of Environmental and Materials Engineering, Nagoya Institute of Technology, Nagoya 466-8555, Japan
Hiroyuki Matsubara
Affiliation:
Department of Environmental and Materials Engineering, Nagoya Institute of Technology, Nagoya 466-8555, Japan
Kazuko Fukutani
Affiliation:
Department of Environmental and Materials Engineering, Nagoya Institute of Technology, Nagoya 466-8555, Japan
Hideto Yoshida
Affiliation:
Department of Earth and Planetary Science, Graduate School of Science, The University of Tokyo, Tokyo 113-0033, Japan
Corresponding

Abstract

X-ray powder diffraction data for a new calcium zirconium phosphate Ca7Zr(PO4)6 are reported. The sample was prepared by heating mixtures of CaCO3, ZrO2, and NH4H2PO4 in prescribed molar ratios at 1623 K. Powder diffraction data were collected with a laboratory X-ray source (Cu Kα) for refinement of unit-cell parameters and intensity measurement of individual reflections. Crystallographic data were Ca7Zr(PO4)6, cubic, I-43d (No. 220), a=0.98338(1) nm, V=0.95097(3) nm3, Z=2, and Dx=3.29 Mg m−3. This compound is most probably isomorphous with eulytite.

Type
New Diffraction Data
Copyright
Copyright © Cambridge University Press 2004

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References

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