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On the determination of reduced Young's modulus and hardness of elastoplastic materials using a single sharp indenter

Published online by Cambridge University Press:  01 January 2006

Yan Ping Cao*
Affiliation:
Laboratoíre des Systèmes Mécaniques et d’ingénierie Simultanée, FRE, CNRS 2719, Université de technologie de Troyes, 10010 Troyes, France
Xiu Qing Qian
Affiliation:
Department of Engineering Mechanics, Tsinghua University, Beijing 100084, People's Republic of China
Jian Lu
Affiliation:
Laboratoíre des Systèmes Mécaniques et d’ingénierie Simultanée, FRE, CNRS 2719, Université de technologie de Troyes, 10010 Troyes, France
*
a)Address all correspondence to this author. e-mail: cypqjl@yahoo.com
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Abstract

In this work, we analyzed the theoretical errors of reduced Young's modulus and hardness of materials provided by single sharp indenter algorithms. According to the analysis, two conclusions can be drawn. First, various methods that use only the indentation loading and unloading curves from a single sharp indenter and omit the effect of the strain hardening exponent own the same widths of the theoretical error bands defined here. They are WEb for reduced Young's modulus and WHb for hardness. Second, the upper-bounds, BUE and BUH, and lower-bounds, BLE and BLH, of theoretical errors of the measured reduced Young's modulus and hardness might be different for different methods. These conclusions, on the one hand, are relevant to the evaluation of various established single sharp indenter algorithms. On the other hand, they provide useful information (i.e., to optimize the theoretical error bounds) for correcting an established method and the development of new single sharp indenter algorithms. According to the conclusions, an energy-based method has been devised to determine reduced Young's modulus and hardness of materials from nanoindentation tests using a standard Berkovich or Vickers indenter (equivalent to a 70.3° cone). It has been shown that the present method owns the reasonable theoretical error bounds and can provide stable results in the presence of data errors.

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Articles
Copyright
Copyright © Materials Research Society 2006

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References

REFERENCES

1.Tabor, D.: Indentation hardness: Fifty years on–A personal view.experiments. Philos. Mag. A 74, 1207 (1996).CrossRefGoogle Scholar
2.Oliver, W.C. and Pharr, G.M.: An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments. J. Mater. Res. 7, 1564 (1992).CrossRefGoogle Scholar
3.Doener, M.F. and Nix, W.D.: A method for interpreting the data from depth-sensing indentation instruments. J. Mater. Res. 1, 601 (1986).CrossRefGoogle Scholar
4.Suresh, S. and Giannakopoulos, A.E.: A new method for estimating residual stresses by instrumented sharp indentation. Acta Mater. 46, 5755 (1998).CrossRefGoogle Scholar
5.Carlsson, S. and Larsson, P.L.: On the determination of residual stress and strain fields by sharp indentation testing: Part I. Theoretical and numerical analysis. Acta Mater. 49, 2179 (2001).CrossRefGoogle Scholar
6.Carlsson, S. and Larsson, P.L.: On the determination of residual stress and strain fields by sharp indentation testing: Part II. Experimental investigation. Acta Mater. 49, 2193 (2001).CrossRefGoogle Scholar
7.Swadener, J.G., Taljat, B. and Pharr, G.M.: Measurement of residual stress by load and depth-sensing indentation with spherical indenters. J. Mater. Res. 16, 2091 (2001).CrossRefGoogle Scholar
8.Dao, M., Chollacoop, N., Van Vliet, K.J., Venkatesh, T.A. and Suresh, S.: Computational modelling of the forward and reverse problems in instrumented sharp indentation. Acta Mater. 49, 3899 (2001).CrossRefGoogle Scholar
9.Bucaille, J.L., Stauss, S., Felder, E. and Michler, J.: Determination of plastic properties of metals by instrumented indentation using different sharp indenters. Acta Mater. 51, 1663 (2003).CrossRefGoogle Scholar
10.Cao, Y.P., Qian, X.Q., Lu, J. and Yao, Z.H.: An energy-based method to extract plastic properties of metal materials from conical indentation tests. J. Mater. Res. 20, 1194 (2005).CrossRefGoogle Scholar
11.Wang, L.G., Ganor, M. and Rokhlin, S.I.: Inverse scaling functions in nanoindentation with sharp indenters: Determination of material properties. J. Mater. Res. 20, 987 (2005).CrossRefGoogle Scholar
12.Nakamura, T., Wang, T. and Sampath, S.: Determination of properties of graded materials by inverse analysis and instrumented indentation. Acta Mater. 48, 4293 (2000).CrossRefGoogle Scholar
13.Bolshakov, A. and Pharr, G.M.: Influences of pileup on the measurement of mechanical properties by load and depth-sensing indentation techniques. J. Mater. Res. 13, 1049 (1998).CrossRefGoogle Scholar
14.Xu, Z.H. and Agren, J.: An analysis of piling-up or sinking-in behaviour of elastic–plastic materials under a sharp indentation. Philos. Mag. 84, 2367 (2004).CrossRefGoogle Scholar
15.Cheng, Y.T. and Cheng, C.M.: Relationships between hardness, elastic modulus, and the work of indentation. Appl. Phys. Lett. 73, 614 (1998).CrossRefGoogle Scholar
16.Oliver, W.C. and Pharr, G.M.: Measurement of hardness and elastic modulus by instrumented indentation: Advances in understanding and refinement to methodology. J. Mater. Res. 19, 3 (2004).CrossRefGoogle Scholar
17.Alkorta, J., Martínez-Esnaola, J.M. and Sevillano, J. Gil: Absence of one-to-one correspondence between elastoplastic properties and sharp-indentation load–penetration data. J. Mater. Res. 20, 432 (2005).CrossRefGoogle Scholar
18.Sakai, M.: Simultaneous estimate of elastic/plastic parameters in depth-sensing indentation tests. Scripta Mater. 51, 391 (2004).CrossRefGoogle Scholar
19.Ma, D.J., Ong, C.W. and Wong, S.F.: New relationship between Young's modulus and nonideally sharp indentation parameters. J. Mater. Res. 19, 2144 (2004).CrossRefGoogle Scholar
20.Choi, Y., Lee, H.S. and Kong, D.: Analysis of sharp-tip-indentation load–depth curve for contact area determination taking into account pile-up and sink-in effects. J. Mater. Res. 19, 3307 (2004).CrossRefGoogle Scholar
21.Tho, K.K., Swaddiwudhipong, S., Liu, Z.S., Zeng, K. and Hua, J.: Uniqueness of reverse analysis from conical indentation tests. J. Mater. Res. 19, 2498 (2004).CrossRefGoogle Scholar
22.ABAQUS, Theory Manual Version 6.4 (Hibbitt, Karlsson and Sorensen Inc, Pawtucket, RI, 2004).Google Scholar
23.Hay, J.C., Bolshakov, A. and Pharr, G.M.: A critical examination of the fundamental relations used in the analysis of nanoindentation data. J. Mater. Res. 14, 2296 (1999).CrossRefGoogle Scholar
24.Cao, Y.P. and Lu, J.: Depth-sensing instrumented indentation with dual indenters: Stability analysis and corresponding regularization schemes. Acta Mater. 52, 1143 (2004).CrossRefGoogle Scholar
25.Lanczos, C.: Linear Differential Operators (Van Nostrand, New York, 1961).Google Scholar
26.Bolzon, G., Maier, G. and Panico, M.: Material modelling calibration by indentation, imprint mapping and inverse analysis. Int. J. Solids Struct. 41, 2957 (2004).CrossRefGoogle Scholar
27.Casals, O. and Alcala, J.: The duality in mechanical property extractions from Vickers and Berkovich instrumented indentation experiments. Acta Mater. 53, 3545 (2005).CrossRefGoogle Scholar
28.Swaddiwudhipong, S., Tho, K.K., Liu, Z.S. and Zeng, K.: Material characterization based on dual indenters. Int. J. Solids Struct. 42, 69 (2005).CrossRefGoogle Scholar