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A novel organothermal reduction process for producing nanocrystalline Ni2P with a circular-shaped flake morphology

Published online by Cambridge University Press:  31 January 2011

Shu-Hong Yu ,
Jian Yang ,
Yong-Sheng Wu ,
Zhao-Hui Han ,
Lei Shu ,
Yi Xie  and
Yi-Tai Qian
Shu-Hong Yu*
Affiliation:
Structure Research Laboratory and Department of Chemistry, University of Science and Technology of China, Hefei, 230026, People's Republic of China
Jian Yang
Affiliation:
Department of Chemistry, University of Science and Technology of China, Hefei, 230026, People's Republic of China
Yong-Sheng Wu
Affiliation:
Department of Chemistry, University of Science and Technology of China, Hefei, 230026, People's Republic of China
Zhao-Hui Han
Affiliation:
Department of Chemistry, University of Science and Technology of China, Hefei, 230026, People's Republic of China
Lei Shu
Affiliation:
Department of Chemistry, University of Science and Technology of China, Hefei, 230026, People's Republic of China
Yi Xie
Affiliation:
Department of Chemistry, University of Science and Technology of China, Hefei, 230026, People's Republic of China
Yi-Tai Qian*
Affiliation:
Structure Research Laboratory and Department of Chemistry, University of Science and Technology of China, Hefei, 230026, People's Republic of China
*
a) Address all correspondence to this author.
a) Address all correspondence to this author.
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Extract

An organothermal reduction process has been successfully developed for synthesis of nanocrystalline Ni2P in benzene at 140 °C. An x-ray powder diffraction pattern (XRD) indicated that the product was pure hexagonal Ni2P phase with a cell constants a =0.5866 and c = 0.3377 nm. Transmission electron microscopy (TEM) showed that the average particle size of the powders was 40 nm with a circular-shaped flake morphology.

Type
Articles
Information
Journal of Materials Research , Volume 13 , Issue 12 , December 1998 , pp. 3365 - 3367
Copyright
Copyright © Materials Research Society 1998

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