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Novel method for the synthesis of thin film coatings on particulate materials

Published online by Cambridge University Press:  31 January 2011

J. M. Fitz-Gerald ,
R. K. Singh ,
H. Gao ,
D. Wright ,
M. Ollinger ,
J. W. Marcinka  and
S. J. Pennycook
J. M. Fitz-Gerald
Affiliation:
Naval Research Laboratory, Code 6372, Washington, District of Columbia 20375
R. K. Singh
Affiliation:
Department of Materials Science and Engineering, University of Florida, Gainesville, Florida 32611
H. Gao
Affiliation:
Department of Materials Science and Engineering, University of Florida, Gainesville, Florida 32611
D. Wright
Affiliation:
Department of Materials Science and Engineering, University of Florida, Gainesville, Florida 32611
M. Ollinger
Affiliation:
Department of Materials Science and Engineering, University of Florida, Gainesville, Florida 32611
J. W. Marcinka
Affiliation:
Department of Electrical Engineering, Florida Atlantic University, Boca Raton, Florida 33431
S. J. Pennycook
Affiliation:
Solid State Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831
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Abstract

In this paper, we show the feasibility of the pulsed-laser ablation technique to grow 20–30-nm-thick, discrete and continuous coatings on particulate material systems so that the properties of the core particles can be suitably modified. Experiments were conducted with a pulsed excimer laser (λ = 248 nm, pulse duration = 25 ns) to deposit nanoparticle coatings on Al2O3 and SiO2 core particles by irradiation of Ag and Y2O3–Eu3+ sputtering targets. Structural characterization was performed with scanning electron microscopy, wavelength dispersive x-ray mapping, transmission electron microscopy, and scanning transmission electron microscopy with z-contrast.

Type
Articles
Information
Journal of Materials Research , Volume 14 , Issue 8 , August 1999 , pp. 3281 - 3291
Copyright
Copyright © Materials Research Society 1999

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