Hostname: page-component-848d4c4894-ndmmz Total loading time: 0 Render date: 2024-05-17T17:14:30.164Z Has data issue: false hasContentIssue false
  • English
  • Français

An experimental and modeling investigation of particle production by spray pyrolysis using a laminar flow aerosol reactor

Published online by Cambridge University Press:  31 January 2011

I. Wuled Lenggoro ,
Takeshi Hata ,
Ferry Iskandar ,
Melissa M. Lunden  and
Kikuo Okuyama
I. Wuled Lenggoro
Affiliation:
Department of Chemical Engineering, Hiroshima University, Kagamiyama 1–4–1, Higashi-Hiroshima 739–8527 Japan
Takeshi Hata
Affiliation:
Department of Chemical Engineering, Hiroshima University, Kagamiyama 1–4–1, Higashi-Hiroshima 739–8527 Japan
Ferry Iskandar
Affiliation:
Department of Chemical Engineering, Hiroshima University, Kagamiyama 1–4–1, Higashi-Hiroshima 739–8527 Japan
Melissa M. Lunden
Affiliation:
Environmental Energy Technologies Division, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, Berkeley, California 94720
Kikuo Okuyama*
Affiliation:
Department of Chemical Engineering, Hiroshima University, Kagamiyama 1–4–1, Higashi-Hiroshima 739–8527 Japan
*
a)Address all correspondence to this author. e-mail: okuyama@ipc.hiroshima-u.ac.jp
Get access

Abstract

The influence of operating parameters on the morphology of particles prepared by spray pyrolysis was investigated using a temperature-graded laminar flow aerosol reactor. Experimentally, zirconia particles were prepared by spray pyrolysis using an aqueous solution of zirconyl hydroxide chloride. Hollow particles were formed if the reactor temperature was high, the temperature gradient was too large, the flow rate of carrier gas was high, and the initial solute concentration was low. A numerical simulation of the pyrolysis process was developed using a combination of two previous models. The simulation results compared well with the experimental results.

Type
Articles
Information
Journal of Materials Research , Volume 15 , Issue 3 , March 2000 , pp. 733 - 743
Copyright
Copyright © Materials Research Society 2000

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1.Messing, G.L., Zhang, S.C., and Jayanthi, G.V., J. Am. Ceram. Soc. 76, 2707 (1993).CrossRefGoogle Scholar
2.Tohge, N., Tatsumisago, M., Minami, T., Okuyama, K., Adachi, M., and Kousaka, Y., J. Am. Ceram. Soc. 74, 2112 (1991).Google Scholar
3.Okuyama, K., Lenggoro, I.W., Tagami, N., Tamaki, S., and Tohge, N., J. Mater. Sci. 32, 1229 (1997).CrossRefGoogle Scholar
4.Lenggoro, I.W., Kang, Y.C., Komiya, T., Okuyama, K., and Tohge, N., Jpn. J. Appl. Phys. 37, L288 (1998).CrossRefGoogle Scholar
5.Kang, Y.C., Park, S.B., Lenggoro, I.W., and Okuyama, K., J. Mater. Res. 14, 2611 (1999).CrossRefGoogle Scholar
6.Ranz, W.E. and Marshall, W.R., Chem. Eng. Prog. 48, 141, 173 (1952).Google Scholar
7.Charlesworth, D.H. and Marshall, W.R. Jr, AIChE. J. 6, 9 (1960).Google Scholar
8.Sano, Y. and Keey, R.B., Chem. Eng. Sci. 27, 881 (1982).CrossRefGoogle Scholar
9.Leong, K.H., J. Aerosol Sci. 18, 511 (1987).CrossRefGoogle Scholar
10.Yu, H., Part. Sci. Technol. 13, 149 (1995).Google Scholar
11.Jayanthi, G.V., Zhang, S.C., and Messing, G.L., Aerosol Sci. Technol. 19, 478 (1993).Google Scholar
12.Xiong, Y. and Kodas, T.T., J. Aerosol Sci. 24, 893 (1993).CrossRefGoogle Scholar
13.van der Lijn, J., Agricultural Res. Report No. 845 (1976).Google Scholar
14.Zhang, S.C. and Messing, G.L., in Ceramic Powder Science III, edited by Messing, G.L., Hirano, S., and Hausner, H. (American Ceramic Society, Westerville, OH, 1990), p. 49.Google Scholar
15.Shimada, M., Seto, T., and Okuyama, K., AIChE J. 39, 1859 (1993).CrossRefGoogle Scholar
16.Hinds, W.C., Aerosol Technology (Wiley, New York, 1982).Google Scholar
17.Hindmarsh, A.C. and Byrne, G.D., Lawrence Livermore National Laboratory Report, UCID-30112 (1977).Google Scholar