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Relation between internal boundaries and critical current in textured YBa2Cu3O7−δ: Transmission electron microscope observations

Published online by Cambridge University Press:  31 January 2011

A. Khalfi
Affiliation:
Laboratoire de Matériaux Céramiques et Traitement de Surfaces, E.S.A. C.N.R.S. 6015, 123 avenue Albert Thomas, 87060 Limoges Cedex, France
G. Trolliard
Affiliation:
Laboratoire de Matériaux Céramiques et Traitement de Surfaces, E.S.A. C.N.R.S. 6015, 123 avenue Albert Thomas, 87060 Limoges Cedex, France
B. Soulestin
Affiliation:
Laboratoire de Matériaux Céramiques et Traitement de Surfaces, E.S.A. C.N.R.S. 6015, 123 avenue Albert Thomas, 87060 Limoges Cedex, France
D. S. Smith
Affiliation:
Laboratoire de Matériaux Céramiques et Traitement de Surfaces, E.S.A. C.N.R.S. 6015, 123 avenue Albert Thomas, 87060 Limoges Cedex, France
J. P. Bonnet
Affiliation:
Laboratoire de Matériaux Céramiques et Traitement de Surfaces, E.S.A. C.N.R.S. 6015, 123 avenue Albert Thomas, 87060 Limoges Cedex, France
D. Bourgault
Affiliation:
Elaboration par Procédés Magnétiques, Matériaux et Force Magnétique (MATFORMAG), U.P.R. C.N.R.S. 9033, 25 avenue des Matyrs B.P. 166, 38042 Grenoble Cedex 9, France
R. Tournier
Affiliation:
Elaboration par Procédés Magnétiques, Matériaux et Force Magnétique (MATFORMAG), U.P.R. C.N.R.S. 9033, 25 avenue des Matyrs B.P. 166, 38042 Grenoble Cedex 9, France
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Abstract

The local critical current (Ic) at 77 K measured at the mm scale in a 60 mm long sample of YBa2Cu3O7−δ prepared by a melting zone process is correlated to the microstructure. Lower values of Ic (<20 A) were obtained in a part of the sample which optical microscope examination showed to be generally polycrystalline. In contrast, the rest of the sample, consisting mostly of large textured domains, gave values for Ic of 120 A and above. Transmission electron microscope observations revealed that the textured domains contain internal boundaries. Depending on the scale of observation, the misorientation angles across the boundaries could vary from a few tenths of a degree up to a few degrees. This seems characteristic for boundaries in textured material which allow strong coupling of the superconducting current across themselves.

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Articles
Copyright
Copyright © Materials Research Society 1998

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