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RETREATMENT OF BONE MATERIAL IN THE GLIWICE RADIOCARBON LABORATORY USING ULTRAFILTRATION

Published online by Cambridge University Press:  19 March 2024

Fatima Pawełczyk Open the ORCID record for Fatima Pawełczyk [Opens in a new window] ,
Magdalena Niedziałkowska ,
Sławomira Pawełczyk Open the ORCID record for Sławomira Pawełczyk [Opens in a new window] ,
Natalia Piotrowska Open the ORCID record for Natalia Piotrowska [Opens in a new window]  and
Maciej Sykut
Fatima Pawełczyk*
Affiliation:
Institute of Physics – CSE, Silesian University of Technology, Konarskiego 22B, 44-100 Gliwice, Poland
Magdalena Niedziałkowska
Affiliation:
Mammal Research Institute Polish Academy of Sciences, Stoczek 1, 17-230 Białowieża, Poland
Sławomira Pawełczyk
Affiliation:
Institute of Physics – CSE, Silesian University of Technology, Konarskiego 22B, 44-100 Gliwice, Poland
Natalia Piotrowska
Affiliation:
Institute of Physics – CSE, Silesian University of Technology, Konarskiego 22B, 44-100 Gliwice, Poland
Maciej Sykut
Affiliation:
Mammal Research Institute Polish Academy of Sciences, Stoczek 1, 17-230 Białowieża, Poland
*
*Corresponding author. Email: fatima.pawelczyk@polsl.pl
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Abstract

Preparation of bones for radiocarbon (14C) dating is still quite a challenge for researchers. The methods are being tested and improved, to increase reliability of dating results and to verify the previous ones. In this work, a set of gelatine samples, extracted from Cervus elaphus and Cervus canadensis bones from various sites in Europe and a set of human bones from archaeological sites in Poland were subjected to retreatment using ultrafiltration in Gliwice Radiocarbon Laboratory. The tested samples represent a wide range of ages, from older than 40,000 14C years BP to modern. The prepared material was subjected to the measurement of C/N atomic ratios and 14C dating using the accelerator mass spectrometry (AMS) technique. Also, the stable isotopes (δ13C and δ15N) values were determined. In a few cases ultrafiltration allows to improve gelatine quality for long-stored samples, by increasing the %C and %N as well as decreasing C/Nat ratios. Nevertheless, this effect was not observed for majority of the samples. Remeasurements of long-term stored samples give mostly the same 14C ages for ultrafiltered ones and for those without ultrafiltration.

Keywords

AMS datingbones14Cultrafiltration
Type
Research Article
Information
Radiocarbon , Volume 66 , Issue 1 , February 2024 , pp. 134 - 146
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Copyright
© The Author(s), 2024. Published by Cambridge University Press on behalf of University of Arizona

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