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High precision U/Th dating of the rock paintings at Mt. Huashan, Guangxi, southern China

  • Qing-Feng Shao (a1), Edwige Pons-Branchu (a2), Qiu-Ping Zhu (a3), Wei Wang (a4), Hélène Valladas (a2) and Michel Fontugne (a2)...

Abstract

The rock art and the associated natural scenery at 38 sites located in the Zuojiang River valley, in the southwest of Guangxi Zhuang Autonomous Region, southern China, were inscribed recently on UNESCO’s World Heritage List. The painted panel at the site of Mt. Huashan is probably the largest known rock art panel in the world, consisting of approximately 1900 identifiable figures and occupying an area of approximately 8000 m2. To determine a precise age on the rock art at Mt. Huashan, 56 secondary carbonate layers above and below the paintings were studied for their mineralogy, oxygen, and carbon isotopic compositions and dated by the 230Th/U method. The 230Th/U dating results demonstrate that ages of the rock paintings can be bracketed between 1856±16 and 1728±41yr BP corresponding to the middle to the end of the Eastern Han dynasty (AD 25 to 220). The results imply that the rock painting practices at Mt. Huashan probably lasted more than a century, and the Zuojiang rock art is younger than that at Baiyunwan and Cangyuan in Yunnan Province by 1 to 10 centuries.

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Corresponding author

*Corresponding author at: Key Laboratory of Virtual Geographic Environment (Nanjing Normal University), Ministry of Education, Nanjing 210023, China. E-mail: qingfengshao@njnu.edu.cn (Q.-F. Shao).

References

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Aubert, M., Brumm, A., Ramli, M., Sutikna, T., Saptomo, E.W., Hakim, B., Morwood, M.J., van den Bergh, G.D., Kinsley, L., Dosseto, A., 2014. Pleistocene cave art from Sulawesi, Indonesia. Nature 514, 223227.
Aubert, M., O’Connor, S., McCulloch, M., Mortimer, G., Watchman, A., Richer-LaFleche, M., 2007. Uranium-series dating rock art in East Timor. Journal of Archaeological Science 34, 991996.
Ayalon, A., Bar-Matthews, M., Kaufman, A., 1999. Petrography, strontium, barium and uranium concentrations, and strontium and uranium isotope ratios in speleothems as palaeoclimatic proxies: Soreq Cave, Israel. Holocene 9, 715722.
Bednarik, R., Li, F., 1991. Rock art dating in China: past and future. Artefact 14, 2533.
Cheng, H., Edwards, R.L., Shen, C.-C., Polyak, V.J., Asmerom, Y., Woodhead, J., Hellstrom, J., et al., 2013. Improvements in 230Th dating, 230Th and 234U half-life values, and U–Th isotopic measurements by multi-collector inductively coupled plasma mass spectroscopy. Earth and Planetary Science Letters 371–372, 8291.
Cole, N., Watchman, A., 2005. AMS dating of rock art in the Laura Region, Cape York Peninsula, Australia – protocols and results of recent research. Antiquity 79, 661678.
Corchón, M.S., Garate, D., Rivero, O., Valladas, H., Pons-Branchu, E., Murelaga, X., Ortega, P., Vicente, F.J., 2015. U-series and 14C dating for a newly discovered decorated area in the paleolithic cave of la Pena de Candamo (Asturies, Northern Spain). Journal of Archaeological Science: Reports 3, 371380.
David, B., Barker, B., Petchey, F., Delannoy, J.-J., Geneste, J.-M., Rowe, C., Eccleston, M., Lamb, L., Whear, R., 2013. A 28,000 year old excavated painted rock from Nawarla Gabarnmang, northern Australia. Journal of Archaeological Science 40, 24932501.
Douville, E., Salle, E., Frank, N., Eisele, M., Pons-Branchu, E., Ayrault, S., 2010. Rapid and accurate U-Th dating of ancient carbonates using inductively coupled plasma-quadrupole mass spectrometry. Chemical Geology 272, 111.
Fontugne, M., Shao, Q., Frank, N., Thil, F., Guidon, N., Boeda, E., 2013. Cross-dating (Th/U-14C) of calcite covering prehistoric paintings at Serra da Capivara National Park, Piaui, Brazil. Radiocarbon 55, 11911198.
Ford, D.C., Williams, P.W., 2007. Karst Hydrogeology and Geomorphology. John Wiley and Sons, Chichester, UK.
Garcia-Diez, M., Hoffmann, D.L., Zilhao, J., de las Heras, C., Lasheras, J.A., Montes, R., Pike, A.W.G., 2013. Uranium series dating reveals a long sequence of rock art at Altamira Cave (Santillana del Mar, Cantabria). Journal of Archaeological Science 40, 40984106.
Garnett, E.R., Andrews, J.E., Preece, R.C., Dennis, P.F., 2004. Climate change recorded by stable isotopes and trace elements in a British Holocene tufa. Journal of Quaternary Science 19, 251262.
Genty, D., Massault, M., Gilmour, M., Baker, A., Verheyden, S., Keppens, E., 1999. Calculation of past dead carbon proportion and variability by the comparison of AMS 14C and TIMS U/Th ages on two Holocene stalagmites. Radiocarbon 41, 251270.
Göktürk, O.M., Fleitmann, D., Badertscher, S., Cheng, H., Edwards, R.L., Leuenberger, M, Fankhauser, A., Tüysük, O., Kramers, J., 2011. Climate on the southern Black Sea coast during the Holocene: implications from the Sofular Cave record. Quaternary Science Reviews 30, 24332445.
Goslar, T., Hercman, H., Pazdur, A., 2000. Comparison of U-series and radiocarbon dates of speleothems. Radiocarbon 42, 403414.
Guo, H., Han, R., Huang, H., Lan, R., Xie, R., 2010. Types of weathering of the Huashan rock paintings. In Agnew, N. (Ed.), Conservation of Ancient Sites on the Silk Road: Proceedings of the Second International Conference on Conservation of Grotto Sites, Mogao Grottoes, Dunhuang, People’s Republic of China, June 28–July 3, 2004. Getty Conservation Institute, Los Angeles, pp. 311315.
Hellstrom, J., Pickering, R., 2015. Recent advances and future prospects of the U-Th and U-Pb chronometers applicable to archaeology. Journal of Archaeological Science 56, 3240.
Hellstrom, J.C., McCulloch, M.T., 2000. Multi-proxy constraints on the climatic significance of trace element records from a New Zealand speleothem. Earth and Planetary Science Letters 179, 287297.
Hiess, J., Condon, D.J., McLean, N., Noble, S.R., 2012. 238U/235U systematics in terrestrial uranium-bearing minerals. Science 335, 16101614.
Holmgren, K., Lauritzen, S.-E., Possnert, G., 1994. 230Th234U and 14C dating of a late Pleistocene stalagmite in Lobatse II Cave, Botswana. Quaternary Science Reviews 13, 111119.
Ihlenfeld, C., Norman, M.D., Gagan, M.K., Drysdale, R.N., Maas, R., Webb, J., 2003. Climatic significance of seasonal trace element and stable isotope variations in a modern freshwater tufa. Geochimica et Cosmochimica Acta 67, 23412357.
Kaufman, A., Wasserburg, G.J., Porcelli, D., Bar-Matthews, M., Ayalon, A., Halicz, L., 1998. U-Th isotope systematics from the Soreq cave, Israel and climatic correlations. Earth and Planetary Science Letters 156, 141155.
Lachniet, M.S., Bernal, J.B., Asmerom, Y., Polyak, V., 2012. Uranium loss and aragonite–calcite age discordance in a calcitized aragonite stalagmite. Quaternary Geochronology 14, 2637.
Lojen, S., Trkov, A., Scancar, J., Vazquez-Navarro, J.-A., Cukrov, N., 2009. Continuous 60-year stable isotopic and earth-alkali element records in a modern laminated tufa (Jaruga, river Krka, Croatia): implications for climate reconstruction. Chemical Geology 258, 242250.
Maher, K., Ibarra, D.E., Oster, J.L., Miller, D.M., Redwine, J.L., Reheis, M.C., Harden, J.W., 2014. Uranium isotopes in soils as a proxy for past infiltration and precipitation across the western United States. American Journal of Science 314, 821857.
McDermott, F., Frisia, S., Huang, Y., Longinelli, A., Spiro, B., Heaton, T.H.E., Hawkesworth, C.J., et al., 1999. Holocene climate variability in Europe: evidence from δ18O, textural and extension-rate variations in three speleothems. Quaternary Science Reviews 18, 10211038.
McMillan, E.A., Fairchild, I.J., Frisia, S., Borsato, A., McDermott, F., 2005. Annual trace element cycles in calcite–aragonite speleothems: evidence of drought in the western Mediterranean 1200–1100 yr BP. Journal of Quaternary Science 20, 423433.
Morwood, M.J., Walsh, G.L., Watchman, A.L., 2010. AMS radiocarbon ages for beeswax and charcoal pigments in north Kimberley rock art. Rock Art Research 27, 38.
Noronha, A.L., Johnson, K.R., Hu, C., Ruan, J., Southon, J.R., Ferguson, J.E., 2014. Assessing influences on speleothem dead carbon variability over the Holocene: implications for speleothem-based radiocarbon calibration. Earth and Planetary Science Letters 394, 2029.
Ortega, R., Maire, R., Deve, G., Quinif, Y., 2005. High-resolution mapping of uranium and other trace elements in recrystallized aragonite–calcite speleothems from caves in the Pyrenees (France): implication for U-series dating. Earth and Planetary Science Letters 237, 911923.
Pike, A.W.G., Gilmour, M., Pettitt, P., Jacobi, R., Ripoll, S., Bahn, P., Munoz, F., 2005. Verification of the age of the palaeolithic cave art at Creswell Crags, UK. Journal of Archaeological Science 32, 16491655.
Pike, A.W.G., Hoffmann, D.L., Garcia-Diez, M., Pettitt, P.B., Alcolea, J., De Balbin, R., Gonzalez-Sainz, C., et al., 2012. U-series dating of paleolithic art in 11 caves in Spain. Science 336, 14091413.
Plagnes, V., Causse, C., Fontugne, M., Valladas, H., Chazine, J.-M., Fage, L.-H., 2003. Cross dating (Th/U-14C) of calcite covering prehistoric paintings in Borneo. Quaternary Research 60, 172179.
Pons-Branchu, E., Bourrillon, R., Conkey, M., Fontugne, M., Fritz, C., Gárate, D., Quiles, A., et al., 2014a. U-series dating of carbonate formations overlying paleolithic art: interest and limitations. Bulletin de la Société Préhistorique Française 111, 211224.
Pons-Branchu, E., Douville, E., Roy-Barman, M., Dumont, E., Branchu, P., Thil, F., Frank, N., Bordier, L., Borst, W., 2014b. A geochemical perspective on Parisian urban history based on U–Th dating, laminae counting and yttrium and REE concentrations of recent carbonates in underground aqueducts. Quaternary Geochronology 24, 4453.
Qin, C.L., Fu, G.H., Qin, L.D., 2015. One century of the Luo Yue cultural studies (part 1). [In Chinese.] Guangxi Ethnic Research 124, 9097.
Qin, S.M., Qin, C.L., Lu, M.F., Yu, R.Y., 1987. The Investigation and Study of the Rock Art of the Zuojiang River Valley in Guangxi. [In Chinese.]. Guangxi Ethnic Printing House, Nanning, China.
Quiles, A., Valladas, H., Bocherens, H., Delque-Kolic, E., Kaltnecker, E., van der Plicht, J., Delannoy, J.-J., et al., 2016. A high-precision chronological model for the decorated Upper Paleolithic cave of Chauvet-Pont d’arc, Ardeche, France. Proceedings of the National Academy of Sciences of the United States of America 113, 46704675.
Railsback, B.L., Dabous, A.A., Osmond, J.K., Fleisher, C.J., 2002. Petrographic and geochemical screening of speleothems for U-series dating: an example from recrystallized speleothems from Wadi Sannur Cavern, Egypt. Journal of Cave and Karst Studies 64, 108116.
Ramsey, C.B., 2009. Bayesian analysis of radiocarbon dates. Radiocarbon 51, 337360.
Reimer, P.J., Bard, E., Bayliss, A., Beck, J.W., Blackwell, P.G., Bronk Ramsey, C., Buck, C.E., et al., 2013. IntCal 13 and Marine13 radiocarbon age calibration curves 0–50,000 years cal BP. Radiocarbon 55, 18691887.
Robinson, L.F., Henderson, G.M., Hall, L., Matthews, I., 2004. Climatic control of riverine and seawater uranium-isotope ratios. Science 305, 851854.
Russ, J., Hyman, M., Shafer, H.J., Rowe, M.W., 1990. Radiocarbon dating of prehistoric rock paintings by selective oxidation of organic carbon. Nature 348, 710711.
Russell, W.A., Papanastassiou, D.A., Tombrello, T.A., 1978. Ca isotope fractionation on the Earth and other solar system materials. Geochimica et Cosmochimica Acta 42, 10751090.
Smith, M.A., Watchman, A., Ross, J., 2009. Direct dating indicates a Mid-Holocene age for archaic rock engravings in arid central Australia. Geoarchaeology 24, 191203.
Steelman, K.L., Rowe, M.W., Shirokov, V.N., Southon, J.R., 2002. Radiocarbon dates for pictographs in Ignatievskaya Cave, Russia: Holocene age for supposed Pleistocene fauna. Antiquity 76, 341348.
Stuiver, M., Polach, H.A., 1977. Discussion: reporting of 14C data. Radiocarbon 19, 355363.
Taçon, P.S.C., Aubert, M., Gang, L., Decong, Y., Hong, L., May, S.K., Fallon, S., Ji, X.P., Curnoe, D., Herries, A.I.R., 2012. Uranium-series age estimates for rock art in southwest China. Journal of Archaeological Science 39, 492499.
Tisnérat-Laborde, N., Poupeau, J.J., Tannau, J.F., Paterne, M., 2001. Development of a semi-automated system for routine preparation of carbonate samples. Radiocarbon 43, 299304.
Valladas, H., Cachier, H., Arnold, M., 1990. AMS C-14 dates for the prehistoric Cougnac cave paintings and related bone remains. Rock Art Research 7, 1819.
Valladas, H., Cachier, H., Maurice, P., Bernaldo de Quirost, F., Clottes, J., Cabrera Valdés, V., Uzquiano, P., Arnold, M., 1992. Direct radiocarbon dates for prehistoric paintings at the Altamira, El Castillo and Niaux caves. Nature 357, 6870.
Valladas, H., Clottes, J., Geneste, J.M., Garcia, M.A., Arnold, M., Cachier, H., Tisnerat-Laborde, N., 2001. Palaeolithic paintings: evolution of prehistoric cave art. Nature 413, 479.
Veizer, J., Ala, D., Azmy, K., Bruckschen, P., Buhl, D., Bruhn, F., Carden, G.A.F., et al., 1999. 87Sr/86Sr, δ13C and δ18O evolution of Phanerozoic seawater. Chemical Geology 161, 5988.
Wang, N.S., 1984. An introduction to rock paintings in Yunnan Province (People’s Republic of China). Rock Art Research 1, 7590.
Wang, Y., Cheng, H., Edwards, R.L., He, Y., Kong, X., An, Z., Wu, J., Kelly, M.J., Dykoski, C.A., Li, X., 2005. The Holocene Asian monsoon: links to solar changes and North Atlantic climate. Science 308, 854857.
Watchman, A.L., 1993. Evidence of a 25,000-year-old pictograph in northern Australia. Geoarchaeology 8, 465473.
White, W.B., 1988. Geomorphology and Hydrology of Karst Terrains. Oxford University Press, New York.
Woo, K.S., Choi, D.W., 2006. Calcitization of aragonite speleothems in limestone caves in Korea: diagenetic process in a semiclosed system. Geological Society of America, Special Papers 404, 297306.
Yang, B., Braeuning, A., Johnson, K.R., Shi, Y., 2002. General characteristics of temperature variation in China during the last two millennia. Geophysical Research Letter 29, 1324. http://dx.doi.org/10.1029/2001GL014485.
Yuan, S.X., Chen, T.M., Hu, Y.Q., 1986. 14C ages for the rock paintings at Huashan Mountain, Ningming, Guangxi. [In Chinese.] Guangxi Ethnic Research 4, 2733.
Zhang, H.W., Cai, Y.J., Tan, L.C., Qin, S.J., An, Z.S., 2014. Stable isotope composition alteration produced by the aragonite-to-calcite transformation in speleothems and implications for paleoclimate reconstructions. Sedimentary Geology 309, 114.
Zhou, J., Lundstrom, C.C., Fouke, B., Panno, S., Hackley, K., Curry, B., 2005. Geochemistry of speleothem records from southern Illinois: development of (234 U)/(238U) as a proxy for paleoprecipitation. Chemical Geology 221, 120.

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High precision U/Th dating of the rock paintings at Mt. Huashan, Guangxi, southern China

  • Qing-Feng Shao (a1), Edwige Pons-Branchu (a2), Qiu-Ping Zhu (a3), Wei Wang (a4), Hélène Valladas (a2) and Michel Fontugne (a2)...

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