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X-ray powder diffraction data for methoxmetamine hydrochloride, C14H20ClNO2

Published online by Cambridge University Press:  24 July 2018

Bronislav Jurasek
Affiliation:
Department of Chemistry of Natural Compounds UCT Prague, Technická 5, Prague, 166 28, Czech Republic Forensic Laboratory of Biologically Active Substances UCT Prague, Technická 5, Prague, 166 28, Czech Republic
Martin Babor
Affiliation:
Department of Solid State Chemistry UCT Prague, Technická 5, Prague, 166 28, Czech Republic
Stepan Huber
Affiliation:
Department of Inorganic Chemistry UCT Prague, Technická 5, Prague, 166 28, Czech Republic
Martin Kuchar*
Affiliation:
Department of Chemistry of Natural Compounds UCT Prague, Technická 5, Prague, 166 28, Czech Republic Forensic Laboratory of Biologically Active Substances UCT Prague, Technická 5, Prague, 166 28, Czech Republic
*
a)Author to whom correspondence should be addressed. Electronic mail: kuchara@vscht.cz

Abstract

X-ray powder diffraction data, unit-cell parameters and space group for methoxmetamine (C14H20ClNO2) are reported [a = 6.5768(7) Å, b = 14.0830(10) Å, c = 15.0530(10) Å, β = 90.975(2)°, unit-cell volume V = 1394.0(2) Å3, and Z = 4, and space group P21/n]. All measured lines were indexed and are consistent with the P21/n space group. No detectable impurities were observed.

Type
New Diffraction Data
Copyright
Copyright © International Centre for Diffraction Data 2018 

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References

de Wolff, P. M. (1968). “A simplified criterion for the reliability of a powder pattern,” J. Appl. Crystallogr. 1, 108113.Google Scholar
EMCDDA (2014). Methoxetamine – Report on the Risk Assessment of 2-(3-Methoxyphenyl)-2-(Ethylamino)Cyclohexanone (Methoxetamine) in the Framework of the Council Decision on new Psychoactive Substances (Publications Office of the European Union, Luxembourg, Luxembourg).Google Scholar
EMCDDA (2016). European Drug Markets Report: In-Depth Analysis (Publications Office of the European Union, Luxembourg, Luxembourg).Google Scholar
EMCDDA and Europol (2017). European Drug Report: Trends and Developments (Publications Office of the European Union, Luxembourg, Luxembourg).Google Scholar
Fojtikova, L., Holubova, B., and Kuchar, M. (2017). “New psychoactive substances,” Chem. Listy 111, 234238.Google Scholar
Hondebrink, L., Nugteren-van Lonkhuyzen, J. J., Van Der Gouwe, D., and Brunt, T. M. (2015). “Monitoring new psychoactive substances (NPS) in The Netherlands: data from the drug market and the Poisons Information Centre,” Drug Alcohol Depend. 147, 109115.Google Scholar
Jurasek, B. and Kuchar, M. (2017). “Methoxfenidin,” Drugs Forensics Bull. 23, 37.Google Scholar
Jurasek, B., Himl, M., Jurok, R., Hajkova, K., Vobinuskova, A., Rezanka, P., and Kuchar, M. (2017). “Synthesis of methoxetamine, its metabolites and deuterium labelled analog as analytical standards and their HPLC and chiral capillary electrophoresis separation,” RSC Adv. 7, 5669156696.Google Scholar
Páleníček, T., Lhotková, E., Žídková, M., Balíková, M., Kuchař, M., Himl, M., Mikšatkova, P., Čegan, M., Valeš, K., Tylš, F., and Horsley, R. R. (2016). “Emerging toxicity of 5,6-methylenedioxy-2-aminoindane (MDAI): pharmacokinetics, behaviour, thermoregulation and LD50 in rats,” Prog. Neuropsychopharmacol. Biol. Psychiatry 69, 4959.Google Scholar
Smith, G. S. and Snyder, R. L. (1979). “FN: a criterion for rating powder diffraction pattern and evaluating the reliability of powder indexing,” J. Appl. Crystallogr. 12, 6065.Google Scholar
Stevens, C. L. and Parke, D. (1966). “Aminoketones and methods for their production,” Patent US3254124.Google Scholar
Werner, P. E. (1964). “Trial-and-error computer methods for the indexing of unknown powder patterns,” Z. Kristallogr. – Cryst. Mater. 120, 375387.Google Scholar
Zanda, M. T., Fadda, P., Chiamulera, C., Fratta, W., and Fattore, L. (2016). “Methoxetamine, a novel psychoactive substance with serious adverse pharmacological effects,” Behav. Pharmacol. 27, 489496.Google Scholar
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