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Powder X-ray diffraction of 1-(4-Nitrophenyl)-2-piperidinone, C11H12N2O3

  • Qing Wang (a1), Xin Nuo Xiong (a1), Jia Wei He (a1), Pei Xiao Tang (a1) and Hui Li (a1)...

Abstract

X-ray powder diffraction data for 1-(4-Nitrophenyl)-2-piperidinone, C11H12N2O3, are reported [a = 9.514(3) Å, b = 12.308(6) Å, c = 9.175(1) Å, α = 90°, β = 91.811(2)°, γ = 90°, V = 1073.94 Å3, Z = 4, ρ cal = 1.362 g cm−3 and space group P21/n]. All measured lines were indexed and are consistent with the P21/n space group. No detectable impurities were observed.

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a) Author to whom correspondence should be addressed. Electronic mail: lihuilab@sina.com

References

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Boultif, A. and Louër, D. (1991). “Indexing of powder diffraction patterns for low-symmetry lattices by the successive dichotomy method,” J. Appl. Crystallogr. 24, 987993.
de Wolff, P. M. (1968). “A simplified criterion for the reliability of a powder pattern,” J. Appl. Crystallogr. 1, 108113.
Jiang, J. and Ji, Y. (2013). “Alternate synthesis of apixaban (BMS-562247), an inhibitor of blood coagulation factor Xa,” Synth. Commun. 43(1), 7279.
Pawley, G. S. (1981). “Unit-cell refinement from powder diffraction scans,” J. Appl. Crystallogr. 14(6), 357361.
Smith, G. S. and Snyder, R. L. (1979). “FN: a criterion for rating powder diffraction patterns and evaluating the reliability of powder indexing,” J. Appl. Crystallogr. 12, 6065.
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Powder X-ray diffraction of 1-(4-Nitrophenyl)-2-piperidinone, C11H12N2O3

  • Qing Wang (a1), Xin Nuo Xiong (a1), Jia Wei He (a1), Pei Xiao Tang (a1) and Hui Li (a1)...

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