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Powder diffraction data of two tricydic diazonia diiodide salts used in silver iodide solid electrolytes

Published online by Cambridge University Press:  10 January 2013

J. Estienne
Affiliation:
Laboratoire de Spectrométries et Dynamique Moléculaire, Université de Provence, Centre de Saint-Jérôme, Case 542, 13397, Marseille, France
O. Cerclier
Affiliation:
Centre de Cristallochimie, Université de Provence, Centre Saint Charles, 13003, Marseille, France
J. J. Rosenberg
Affiliation:
Laboratoire de Chimie des Matériaux Inorganiques, Université Paul Sabatier, 118 route de Narbonne 31062, Toulouse Cedex, France

Abstract

Indexed X-ray powder diffraction data are reported for two organic salts with carbon rings having two quaternary nitrogens: diazonia-6,9 dispiro [5.2.5.2] hexadecane and diazonia-6,9 dispiro [5.2.5.3] heptadecane diiodides. For these compounds, which give solid electrolytes when associated with AgI, powder diffraction diagrams calculated by the Rietveld method from single crystal structure determinations are presented and are compared to the experimental diffraction data.

Type
Research Article
Copyright
Copyright © Cambridge University Press 1993

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