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Crystallographic study of PtCl2(C2H3O2)2(C6H13N)(NH3) by Rietveld refinement

Published online by Cambridge University Press:  06 March 2012

Lingmin Zeng ,
Liangwei Chen ,
Shaoping Pu ,
Yikun Yang ,
Wenggui Gao  and
Yao Yu
Lingmin Zeng*
Affiliation:
Institute of Materials Science, Guangxi University, Nanning, Guangxi 530004, People’s Republic of China
Liangwei Chen
Affiliation:
Sino-Platinum Metals Co. Ltd., Kunming 650221, People’s Republic of China
Shaoping Pu
Affiliation:
Institute of Precious Metals, Kunming 650221, People’s Republic of China
Yikun Yang
Affiliation:
Institute of Precious Metals, Kunming 650221, People’s Republic of China
Wenggui Gao
Affiliation:
Institute of Precious Metals, Kunming 650221, People’s Republic of China
Yao Yu
Affiliation:
Institute of Precious Metals, Kunming 650221, People’s Republic of China
*
a)Electronic mail: lmzeng@gxu.edu.cn
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Abstract

X-ray powder diffraction data for the anticancer drug PtCl2(C2H3O2)2(C6H13N)(NH3) are reported. The crystal structure of PtCl2(C2H3O2)2(C6H13N)(NH3) obtained from a Rietveld refinement are: space group P21/a, a=13.547(2) Å, b=8.260(1) Å, c=14.638(3) Å, β=110.429(2)°, V=1534.96 Å3, Z=4 and Dcalc.=2.068 Mg/m3.

Keywords

structure determinationRietveld analysispowder diffractionPtCl2(C2H3O2)2(C6H13N)(NH3)
Type
Technical Articles
Information
Powder Diffraction , Volume 18 , Issue 2 , June 2003 , pp. 140 - 143
Copyright
Copyright © Cambridge University Press 2005

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References

Horwich, A. (1989). Br. J. Cancer BJCAAI 59, 156–159. bjc, BJCAAI CrossRefGoogle Scholar
Kelland, L. R., Murrer, B. A., Abel, G., Giandomenico, C. M., Mistry, P., and Harrap, K. R. (1992). Cancer Res. CNREA8 52, 822–828. cnr, CNREA8 Google Scholar
Kelland, L. R., Abel, G., McKeage, M. J., Jones, M., Goddard, P. M., Valenti, M., Murrer, B. A., and Harrap, K. R. (1993). Cancer Res. CNREA8 53, 2581–2583. cnr, CNREA8 Google Scholar
Marciniak, H. (1997). DMPLOT-Plot view program for Rietveld refinement Method. V3.38.Google Scholar
Materials Data, Inc. (1999). Jade 5, XRD pattern processing.Google Scholar
Neidle, S.and Snook, C. F. (1995). Acta Crystallogr., Sect. C: Cryst. Struct. Commun. ACSCEE 51, 822–824. acg, ACSCEE CrossRefGoogle Scholar
Smith, G. S.and Snyder, R. L. (1979). J. Appl. Crystallogr. JACGAR 12, 60. acr, JACGAR CrossRefGoogle Scholar
Young, R. A., Sakthivel, A., Moss, T. S., and Paiva-Santols, C. O. (1995). “DBWS-9411, an upgrade of DBWS. Programs for Rietveld refinement with PC and mainframe computers,” J. Appl. Crystallogr. JACGAR 28, 366–367. acr, JACGAR CrossRefGoogle Scholar