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X-ray powder diffraction data for potassium erbium fluoride

Published online by Cambridge University Press:  04 September 2013

J. Maixner*
Affiliation:
Central Laboratories, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
V. Bartůněk
Affiliation:
Central Laboratories, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic Department of Inorganic Chemistry, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
*
a)Author to whom correspondence should be addressed. Electronic mail: jaroslav.maixner@vscht.cz

Abstract

X-ray powder diffraction data, unit-cell parameters, and space group for potassium erbium fluoride, K0.5Er0.5F2, are reported [a = 5.6862(5) Å, unit-cell volume V = 183.85 Å3, Z = 4, and space group Fm-3m]. Potassium erbium fluoride is isostructural with a large family of fluorides represented by the mineral fluorite CaF2. All of the measured lines of the title compound were indexed and are consistent with the Fm-3m space group. No detectable impurities were observed.

Type
New Diffraction Data
Copyright
Copyright © International Centre for Diffraction Data 2013 

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References

Aléonard, S., Labeau, M., Le Fur, Y., and Gorius, M. F. (1973). “Etude du system KF-ErF3,” Mater. Res. Bull. 8(6), 605617.Google Scholar
Bartůněk, V., Rak, J., Král, V., and Smrčkova, O. (2011). “Simple one-step preparation of cerium trifluoride nanoparticles,” J. Fluorine Chem. 132(4), 298301.Google Scholar
Bartůněk, V., Jakeš, V., Král, V., and Rak, J. (2012). “Lanthanum trifluoride nanoparticles prepared using ionic liquids,” J. Fluorine Chem. 135, 358361.Google Scholar
Bartůněk, V., Rak, J., Sofer, Z., and Král, V. (2013). “Nano-crystals of various lanthanide fluorides prepared using the ionic liquid bmimPF6 ,” J. Fluorine Chem. 149, 1317.CrossRefGoogle Scholar
Boultif, A. and Louër, D. (2004). “Powder pattern indexing with the dichotomy method,” J. Appl. Crystallogr. 37, 724731.Google Scholar
de Wollf, P. M. (1968). “A simplified criterion for the reliability of a powder pattern,” J. Appl. Crystallogr. 1, 108113.Google Scholar
Gesland, J. Y., Khaidukov, N. M., Kirikova, N. Y., Kirm, M., Krupa, J. C., Makhov, V. N., Ouvarova, T. V., Queffelec, M., and Zimmerer, G. (1999) “VUV emission of stoichiometric Er3+ and Tm3+containing fluoride crystals,” J. Electron. Spectrosc. Relat. Phenom. 101–103, 579582.Google Scholar
ICDD (2012). “Powder Diffraction File,” edited by McClune, Frank, International Centre for Diffraction Data, 12 Campus Boulevard, Newton Square, Pennsylvania, 19073–3272.Google Scholar
Smith, G. S. and Snyder, R. L. (1979). “FN: A criterion for rating powder diffraction patterns and evaluating the reliability of powder indexing,” J. Appl. Crystallogr. 12, 6065.Google Scholar
Zhang, C., Chen, J., Zhou, Y. C., and Li, D. Q. (2008). “Ionic liquid-based “all-in-one” synthesis and photoluminescence properties of lanthanide fluorides,” J. Phys. Chem. C 112(27), 1008310088.Google Scholar