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Phenylation of Fullerene-C60

  • Roger Taylor (a1), Anthony G. Avent (a1), Paul R. Birkett (a1), Jon C. Crane (a1), Adam D. Darwish (a1), G. John Langley (a1), Harold W. Kroto (a1) and David R. M. Walton (a1)...

Abstract

C60 Cl6 can be phenylated and arylated to give derivatives of the type C60Ar5Cl, which may be readily converted to C60Ar5. The compounds C60Ar5 and various other phenylated derivatives have been isolated from the product of reaction of [60]fullerene with bromine/ferric chloride/benzene, and partially characterised.

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1. Taylor, R., Electrophilic Aromatic Substitution. (Wiley, Chichester, 1989), pp. 202203.
2. Hoke, S. H., Molstad, J., Payne, G. L., Kahr, B., Ben-Amotz, D., and Cooks, R. G., Rapid Comm. Mass Spectr. 5, 472 (1991).
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5. Darwish, A. D. and Taylor, R., unpublished work.
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8. Taylor, R., Langley, G. J., Meidine, M. F., Parsons, J. P., Abdul-Sada, A. K., Dennis, T. J., Hare, J. P., Kroto, H. W., and Walton, D. R. M., J. Chem. Soc., Chem. Commun., 1992 667.
9. Birkett, P. R., Hitchcock, P. B., Kroto, H. W., Taylor, R., and Walton, D. R. M., Nature, 357, 479 (1992).
10. Avent, A. G., Birkett, P. R., Crane, J. D., Darwish, A. D., Langley, G. J., Kroto, H. W., Taylor, R., and Walton, D. R. M., J. Chem. Soc., Perkin Trans. 2, 1994, in press.
11. Taylor, R., J. Chem. Soc., Perkin Trans. 2, 1992 1667.
12. Ref. 1, pp. 432433.
13. Ref 1, Chapter 10.

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