Hostname: page-component-8448b6f56d-42gr6 Total loading time: 0 Render date: 2024-04-16T09:49:40.905Z Has data issue: false hasContentIssue false

Focused ion beam microscope as an analytical tool for nanoscale characterization of gradient-formulated polymeric sensor materials

Published online by Cambridge University Press:  26 February 2011

Katharine Dovidenko
Affiliation:
dovidenk@research.ge.com, GE Global Research Center, 1 Research Circle, Niskayuna, NY, 112309, United States
Radislav A. Potyrailo
Affiliation:
potyrailo@crd.ge.com, GE Global Research Center, United States
Games Grande
Affiliation:
grande@crd.ge.com, GE Global Research Center, United States
Get access

Abstract

In this study, we are demonstrating localized nano-scale analysis of sensor materials which are developed using combinatorial gradient approach. Our technique based on Focused Ion Beam cross-sectioning at specific locations affords establishing metal nano-particles concentrations at best-performing area(s) of gradient-formulated polymer samples. We have achieved three-dimensional characterization/mapping of nano-fillers (30-100 nm metal particles) in composite thin films on variety of substrates.

Type
Research Article
Copyright
Copyright © Materials Research Society 2006

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1. Potyrailo, R. A., Angew. Chem. Int. Ed. 2006, in press; Xia, Y.; Rogers, J. A.; Paul, K. E.; Whitesides, G. M., Chem. Rev. 1999, 99, 18231848].Google Scholar
2. Gianuzzi, L.A. and Steveie, F.A., Editors, Introduction to Focused Ion Beams. Instrumentation, Theory Techniques and Practice, Springer, NY (2005)Google Scholar
3. Lee, E. at all, Microsc.Microanal. 10 (supp12) 1128–29 (2004)Google Scholar
4. Potyrailo, R. A.; Hassib, L., Proceedings of TRANSDUCERS'05, The 13th International Conference on Solid-State Sensors, Actuators and Microsystems, Seoul, Korea, June 5–9, 2005, 20992102 (2005)Google Scholar
5. Potyrailo, R. A.; Hassib, L., Rev. Sci. Instrum. 76, 062225 (2005)Google Scholar
6. Elghanian, R.; Storhoff, J. J.; Mucic, R. C.; Letsinger, R. L.; Mirkin, C. A., Science 277, 10781081 (1997)Google Scholar