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Determination of Hydrogen in Metals, Semiconductors, and Other Materials by Cold Neutron Prompt Gamma-Ray Activation Analysis

Published online by Cambridge University Press:  10 February 2011

R. L. Paul
Affiliation:
Analytical Chemistry Division, National Institute of Standards and Technology, Gaithersburg, MD 20899
R. M. Lindstrom
Affiliation:
Analytical Chemistry Division, National Institute of Standards and Technology, Gaithersburg, MD 20899
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Abstract

Cold neutron prompt gamma-ray activation analysis has proven useful for nondestructive measurement of trace hydrogen. The sample is irradiated in a beam of neutrons; the presence of hydrogen is confirmed by the emission of a 2223 keV gamma-ray. Detection limits for hydrogen are 3 mg/kg in quartz and 8 mg/kg in titanium. We have used the technique to measure hydrogen in titanium alloys, germanium, quartz, fullerenes and their derivatives, and other materials.

Type
Research Article
Copyright
Copyright © Materials Research Society 1998

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