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Continuous Flow Hyper-Polarized 129Xe-Mas Nmr Studies of Microporous Materials.

Published online by Cambridge University Press:  10 February 2011

Andrei Nossov ,
Flavien Guenneau ,
Marie-Anne Springuel-Huet ,
Valérie Montouillout ,
Jean-Pierre Cognec ,
Benno Knott ,
Frank Engelke ,
Antoine Gédéon  and
Christian Fernandez
Andrei Nossov
Affiliation:
Laboratoire Systèmes Interfaciaux á l'Echelle Nanométrique.Université Pierre et Marie Curie, CNRS/Université Pierre et Marie Curie, 4, place jussieu, 75252 Paris, France
Flavien Guenneau
Affiliation:
Laboratoire Systèmes Interfaciaux á l'Echelle Nanométrique.Université Pierre et Marie Curie, CNRS/Université Pierre et Marie Curie, 4, place jussieu, 75252 Paris, France
Marie-Anne Springuel-Huet
Affiliation:
Laboratoire Systèmes Interfaciaux á l'Echelle Nanométrique.Université Pierre et Marie Curie, CNRS/Université Pierre et Marie Curie, 4, place jussieu, 75252 Paris, France
Valérie Montouillout
Affiliation:
Laboratoire Catalyse et Spectrochimie, CNRS/Ensi Caen, 6 bd du Maréchal Juin, 14050 Caen, France
Jean-Pierre Cognec
Affiliation:
Laboratoire Catalyse et Spectrochimie, CNRS/Ensi Caen, 6 bd du Maréchal Juin, 14050 Caen, France
Benno Knott
Affiliation:
Bruker Elektronik GmbH, Silberstreifen, D-76287 Rheinstetten, Germany
Frank Engelke
Affiliation:
Bruker Elektronik GmbH, Silberstreifen, D-76287 Rheinstetten, Germany
Antoine Gédéon
Affiliation:
Laboratoire Systèmes Interfaciaux á l'Echelle Nanométrique.Université Pierre et Marie Curie, CNRS/Université Pierre et Marie Curie, 4, place jussieu, 75252 Paris, France
Christian Fernandez
Affiliation:
Laboratoire Catalyse et Spectrochimie, CNRS/Ensi Caen, 6 bd du Maréchal Juin, 14050 Caen, France
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Summary:

A Magic Angle Spinning (MAS) NMR probe has been designed allowing the in-situ measurements of NMR spectra of working catalyst. The probe was built following the original design of M. Hunger [Hunger, 1995 #2]. It allows the magic angle spinning of powder samples up to 3.5 kHz, under gas flowing conditions, and at temperatures up to 573K.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 775: Symposium P – Self-Assembled Nanostructured Materials , 2003 , P3.20
Copyright
Copyright © Materials Research Society 2003

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