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Cobalt As A Probe Ion In The Synthesis Of CoAPO-5

  • M. G. Uytterhoeven (a1), W. A. Van Keyenberg (a1), R. A. Schoonheydt (a1) and K. U. Leuven (a1)

Abstract

Diffuse reflectance spectroscopy (DRS) is an excellent technique for the investigation of the synthesis process of CoAPO-5. The DRS intensities increase concomitantly with the crystallinity during synthesis. DRS is also useful in the characterization of the nucleation stage. The transition from an aluminophosphate-hydrate to a non-hydrated structure is observed.

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1. Schoonheydt, R.A., Vos, R. de, Pelgrims, J., Leeman, H., in Zeolites: Facts, Figures, Future, Studies in Surface Science and Catalysis 49, edited by Jacobs, P.A. and Santen, R. A. van, (Elsevier, Amsterdam), 559568 (1989)
2. Wilson, S.T. and Flanigen, E.M., US patent, 4 567,029 (28 January 1986)
3. Ballmoos, R. von, Higgins, J.B., Zeolites 10, 331S (1990)
4. Jacobs, P.A., Derouane, E.G. and Weitkamp, J., J.C.S. Chem. Comm., 1981, 591593
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6. Cardile, C.M., Tapp, N.J. and Milestone, N.B., Zeolites 10, 90 (1990)

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