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Atomic-Resolution Electron Microscopy of TiB2 Precipitates in an Industrial TiAl Alloy

Published online by Cambridge University Press:  10 February 2011

B. J. Inkson
Affiliation:
Max-Planck-Institut für Metallforschung, Seestrasse 92, D-70174 Stuttgart, Germany.
G. Möbus
Affiliation:
Max-Planck-Institut für Metallforschung, Seestrasse 92, D-70174 Stuttgart, Germany.
M. Rühle
Affiliation:
Max-Planck-Institut für Metallforschung, Seestrasse 92, D-70174 Stuttgart, Germany.
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Abstract

TiB2 nano-lamellae, grown in-situ within a TiAl intermetallic melt, have been examined by high resolution electron microscopy. The use of the Stuttgart ARM enables Ti and B columns to be distinguished in the HREM images. Examination of the internal structure of the T1B2 platelets reveals extensive prismatic faulting on {1010}TiB2, {0110}TiB2 and {1100}TiB2 planes. Externally, the TiB2 platelets exhibit an orientational relationship {1010}TiB2 // {001}B2 and [0001]TiB2 // <010>B2 with interleaving platelets of B2-phase, with the predominating interface planes being {1010}TiB2 // {001}B2. The minor facets of the TiB2 platelets are [0001]TiB2 // <010>B2. {0110}TiB2 and {1100}TiB2, with the latter two facets showing no relationship with the interleaving B2-phase. No preferred orientation relationship of the TiB2 with the surrounding γ-TiAl and α2-Ti3Al phases is observed.

Type
Research Article
Copyright
Copyright © Materials Research Society 1997

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References

REFERENCES

1. De Graef, M. et al Acta metall. mater. 40, 12, 3395 (1992).Google Scholar
2. Hyman, M.E. et al, Metall. Trans. 20A, 1847 (1989).Google Scholar
3. Inkson, B.J. et al, Journal de phys. IV, Coll. C7, 1, 397 (1993).Google Scholar
4. Inkson, B.J., Boothroyd, C.B. and Humphreys, C., Acta Metall. Mater. 43, 4, 1429 (1995).Google Scholar
5. Inkson, B.J. and Rühle, M., in preparation.Google Scholar