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Synthesis And Characterization Of Nine Metal Nitrides

Published online by Cambridge University Press:  10 February 2011

Travis Wade  and
Richard M. Crooks
Travis Wade
Affiliation:
Department of Chemistry, Texas A & M University, College Station, TX 77843-3255
Richard M. Crooks
Affiliation:
Department of Chemistry, Texas A & M University, College Station, TX 77843-3255
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Abstract

We demonstrate a simple electrochemical method suitable for preparing precursors for nine different metal-nitride ceramics. These precursor powders were calcined in flowing NH3 or Ar to yield metal-nitride ceramic powders. This electrochemical synthetic technique was applied to Al, Ga, Mo, Nb, Ni, Ti, V, W, and Zr and resulted in a nitride of each of these metals. The calcination conditions determined the resulting phase, composition, and morphology of the product. The ceramic materials were characterized primarily by powder XRD.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 410: Symposium S – Covalent Ceramics III-Science and Technology of Non-Oxides , 1995 , 121
Copyright
Copyright © Materials Research Society 1996

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