Hostname: page-component-77c89778f8-9q27g Total loading time: 0 Render date: 2024-07-23T08:40:47.750Z Has data issue: false hasContentIssue false

Characterization of the High Temperature Dislocation Substructure of Mosi2

Published online by Cambridge University Press:  22 February 2011

J. P. Campbell
Affiliation:
Department of Materials Science and EngineeringThe University of Michigan, Ann Arbor, MI 48109–2136
H. Chang
Affiliation:
Department of Materials Science and EngineeringThe University of Michigan, Ann Arbor, MI 48109–2136
R. Gibala
Affiliation:
Department of Materials Science and EngineeringThe University of Michigan, Ann Arbor, MI 48109–2136
Get access

Abstract

The dislocation substructure of polycrystalline MoSi2 deformed in compression at temperatures ranging from 900°C to 1300°C has been investigated. Slip is found to occur primarily by <100> Burgers vectors. A quantitative characterization of the <100> dislocation substructure is developed for several deformation temperatures, including the slip systems present and the relative occurrence of each. Orientation distributions showing the screw/edge character of the <100> dislocations are generated at each deformation temperature. Variations in these distributions with temperature are noted, and the implications of these variations to the deformation behavior of MoSi2 are discussed. Notable observations include the onset of dislocation climb between 900°C and 1100°C, a strong preference for dislocations of mixed character at 900°C, and the complete absence of pure screw dislocations from 900°C to 1300°C.

Type
Research Article
Copyright
Copyright © Materials Research Society 1995

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

1. Vahldiek, F. W. and Mersol, S. A., J. Less-Common Metals, 15, 165 (1968).Google Scholar
2. Umakoshi, Y., Sakagami, T., Hirano, T. and Yamane, T., Acta Metall. Mater., 38, 909 (1990).Google Scholar
3. Boldt, P. H., Embury, J. D. and Weatherly, G. C., Mat. Sci. Eng., A155, 251 (1992).Google Scholar
4. Maloy, S. A., Ph.D. Thesis, Case Western Reserve University, 1994.Google Scholar
5. Unal, O., Petrovic, J. J., Carter, D. H. and Mitchell, T. E., J. Am. Ceram. Soc, 73, 1752 (1990).Google Scholar
6. Mitchell, T. E., Castro, R. G., Petrovic, J. J., Maloy, S. A., Unal, O. and Chadwick, M. M., Mat. Sci. Eng., A155. 241 (1992).Google Scholar
7. Chang, H. and Gibala, R., in High Temperature Ordered Intermetallic Alloys V, ed. by Baker, I., Darolia, R., Whittenberger, J. D. and Yoo, M. H. (Mat. Res. Soc. Symp. Proc. 288, Pittsburgh, PA, 1993) 1143.Google Scholar
8. Maloy, S. A., Heuer, A. H., Lewandowski, J. J. and Mitchell, T. E., Acta Metall. Mater., 40, 3159 (1992).Google Scholar
9. Kung, H., Basu, A. and Ghosh, A. K., to be published.Google Scholar
10. Chang, H. and Gibala, R., in High Temperature Silicides and Refractory Alloys, ed. by Briant, C. L., Petrovic, J. J., Bewlay, B. P., Vasudevan, A. K. and Lipsitt, H. A. (Mat. Res. Soc. Symp. Proc. 322, Pittsburgh, PA, 1994) 223.Google Scholar
11. Ghosh, A. K. and Basu, A., Critical Issues in the Development of High Temperature Structural Materials, ed. by Stoloff, N. S., Duquette, D. J. and Giamei, A. F. (TMS, Warrendale, PA, 1993) 291.Google Scholar
12. Campbell, J. P., Chang, H. and Gibala, R., to be published.Google Scholar