Hostname: page-component-76fb5796d-5g6vh Total loading time: 0 Render date: 2024-04-26T05:04:14.921Z Has data issue: false hasContentIssue false

The Use of Phase and Amplitude Information of Reconstructed Exit Waves

Published online by Cambridge University Press:  02 July 2020

H.W. Zandbergen*
Affiliation:
National Centre for HREM, Laboratory of Materials Science, Delft University of Technology, Rotterdamseweg 137, 2628ALDelft, The Netherlands
Get access

Extract

Exit waves can be reconstructed from through focus series of HREM images or by off-axis holography [1]. We have applied the through focus method to reconstruct exit waves, using algorithms developed by Van Dyck and Coene [2]. Electron microscopy was performed with a Philips CM30ST electron microscope with a field emission gun operated at 300 kV. The high resolution images were recorded using a Tietz software package and a 1024x1024 pixel Photometrix CCD camera having a dynamic range of 12 bits. The reconstructions were done using 15-20 images with focus increments of 5.2 nm. The resulting exit waves were corrected posteriorly for the three fold astigmatism.

The exit wave is complex; consequently it contains phase and amplitude. Since in the very thin regions the specimen acts as a thin phase object, such a thin area will show little contrast, an example of which is shown in Figure 1.

Type
Electron Crystallography; The Electron Phase Problem
Copyright
Copyright © Microscopy Society of America 1997

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

1.Van Dyck, D., Lichte, H. and Van der Mast, K.D., Ultramicroscopy 64, 1 (1996)10.1016/0304-3991(96)00057-5CrossRefGoogle Scholar
2.Coene, W.M.J., Thust, A., Op De Beeck, M., Van Dyck, D., Ultramicroscopy 64, 107 (1996)10.1016/0304-3991(96)00010-1CrossRefGoogle Scholar
3.Jansen, J., D. Tang, , Zandbergen, H.W. and Schenk, H., submitted to Acta Cry st A.Google Scholar
4.Zandbergen, H.W., Tang, D., Jansen, J. and Cava, R.J., Ultramicroscopy 64, 231 (1996)10.1016/0304-3991(96)00015-0CrossRefGoogle Scholar