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Quantitative Energy-filtering Transmission Electron Microscopy in Materials Science

Published online by Cambridge University Press:  19 June 2008

Werner Grogger
Affiliation:
Research Institute for Electron Microscopy, Graz University of Technology
Ferdinand Hofer
Affiliation:
Research Institute for Electron Microscopy, Graz University of Technology
Peter Warbichler
Affiliation:
Research Institute for Electron Microscopy, Graz University of Technology
Gerald Kothleitner
Affiliation:
Research Institute for Electron Microscopy, Graz University of Technology
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Abstract

Energy-filtered transmission electron microscopy (EFTEM) can be used to acquire elemental distribution images at high lateral resolution within short acquisition times. In this article, we present an overview of typical problems from materials science which can be preferentially solved by means of EFTEM. In the first example, we show how secondary phases in a steel specimen can be easily detected by recording jump ratio images of the matrix element under rocking beam illumination. Secondly, we describe how elemental maps can be converted into concentration maps. A Ba-Nd-titanate ceramics serves as a typical materials science example exhibiting three different compounds with varying composition.

Type
Articles
Copyright
2000 Microscopy Society of America

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