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 This work was supported by Joint Center for Energy Storage Research (JCESR), an Energy Innovation Hub funded by the Department of Energy, Office of Science, Basic Energy Sciences (BES). The development of the operando stage was supported by the Chemical Imaging Initiative (CII), a Laboratory Directed Research and Development (LDRD) Program at Pacific Northwest National Laboratory (PNNL). The image analytics used for quantification were developed as part of the Analytics In Motion (AIM) Initiative LDRD Program at PNNL. PNNL is a multi-program national laboratory operated by Battelle for the U.S. Department of Energy (DOE) under Contract DE-AC05-76RL01830. A portion of the research was performed using the Environmental Molecular Sciences Laboratory (EMSL), a national scientific user facility sponsored by the Department of Energy's Office of Biological and Environmental Research and located at PNNL.