Hostname: page-component-77c89778f8-swr86 Total loading time: 0 Render date: 2024-07-16T23:13:53.322Z Has data issue: false hasContentIssue false

Compound Standards For Light Element Eds In Aem, Sem And Lvsem

Published online by Cambridge University Press:  02 July 2020

E D Boyes*
Affiliation:
DuPont Company, CR&D, PO Box 80356-383, Wilmington, DE19880-0356, USA
Get access

Extract

For a number of years we have used in our laboratory a simple extension to light elements of the classical ClifF-Lorimer approach using stoichiometric compound standards containing pairs of heavier elements to determine independently the EDS detector sensitivity contribution to quantitative analysis in the AEM. It is now also extended to direct light element LVEDS analysis in the SEM at low voltage (<5kV). This approach may be more practical, accessible and easily reproducible for routine use than the elegant custom thin film fabrications reported by Egerton, but the latter method has other substantial advantages, including well defined thicknesses, in the most sophisticated applications. As the types of advanced materials have expanded to include ceramics and polymers the requirements for analysis have also changed. In many cases the light elements are now the majority species in advanced materials and the corrections based on older standards are huge; and therefore inevitably rather limited in accuracy.

Type
Quantitative X-Ray Microanalysis
Copyright
Copyright © Microscopy Society of America

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Cliff, G and Lorimer, G,J of Microscopy, 103 (1975), 203CrossRefGoogle Scholar
Egerton, R F and Malac, MProc MSA, 56(1998)230Google Scholar
Goldstein, J et al, SEM and X-ray Microanalysis, Plenum,1981Google Scholar
Boyes, ED, Proc ICEM-12, Paris, 1994, 51Google Scholar
Boyes, ED, Proc EMSA, 50 (1992) 1630Google Scholar