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An Integrated Workflow To Investigate Electrocatalytic Surfaces By Correlative X-ray Photoemission Spectroscopy, Scanning Photoemission Electron Microscopy and Atom Probe Tomography

Published online by Cambridge University Press:  05 August 2019

Kevin Schweinar*
Affiliation:
Max-Planck-Institut für Eisenforschung GmbH, Microstructure Physics and Alloy Design, Düsseldorf, Germany
Olga Kasian
Affiliation:
Max-Planck-Institut für Eisenforschung GmbH, Interface Chemistry and Surface Engineering, Düsseldorf, Germany
Rachel L. Nicholls
Affiliation:
Max-Planck-Institut für Chemische Energiekonversion, Heterogeneous Reactions, Mülheim a.d. Ruhr, Germany
Catherine R. Rajamathi
Affiliation:
Max-Planck-Institut für Chemische Energiekonversion, Heterogeneous Reactions, Mülheim a.d. Ruhr, Germany
Patrick Zeller
Affiliation:
Elettra – Sincrotrone Trieste S.C.p.A., Trieste, Italy
Matteo Amati
Affiliation:
Elettra – Sincrotrone Trieste S.C.p.A., Trieste, Italy
Luca Gregoratti
Affiliation:
Elettra – Sincrotrone Trieste S.C.p.A., Trieste, Italy
Dierk Raabe
Affiliation:
Max-Planck-Institut für Eisenforschung GmbH, Microstructure Physics and Alloy Design, Düsseldorf, Germany
Mark Greiner
Affiliation:
Max-Planck-Institut für Chemische Energiekonversion, Heterogeneous Reactions, Mülheim a.d. Ruhr, Germany
Baptiste Gault
Affiliation:
Max-Planck-Institut für Eisenforschung GmbH, Microstructure Physics and Alloy Design, Düsseldorf, Germany Imperial College, Royal School of Mines, Department of Materials, London, SW7 2AZ, UK
*
*Corresponding author: k.schweinar@mpie.de

Abstract

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Type
Recent Developments in Atom Probe Tomography
Copyright
Copyright © Microscopy Society of America 2019 

References

[1]Li, T et al. , Nat. Catalysis 1 (2018), p. 300-305Google Scholar
[2]Kasian, O et al. , J. Electrochem. Soc. 163 (2016), F3099-F3104Google Scholar
[3]Amati, M et al. , Surf. Science 652 (2016), p. 20-25Google Scholar
[4]The authors wish to thank Elettra Sincrotrone for the allocation of beamtime at the ESCAmicroscopy beamline. The research leading to these results has received funding from the European Community's Horizon 2020 Framework Programme under grant agreement n° 730872. K.S. acknowledges IMPRS-SurMat for funding. U. Tezins and A. Sturm are acknowledged for their technical support at MPIE.Google Scholar