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Results from a New Fast, High Sensitivity, Eels Spectrometer

Published online by Cambridge University Press:  02 July 2020

C. Trevor
Affiliation:
Gatan Research and Development, 5933 Coronado Lane, Pleasanton, CA94588
R. Harmon
Affiliation:
Gatan Research and Development, 5933 Coronado Lane, Pleasanton, CA94588
H. Brink
Affiliation:
Gatan Research and Development, 5933 Coronado Lane, Pleasanton, CA94588
J. Hunt
Affiliation:
Gatan Research and Development, 5933 Coronado Lane, Pleasanton, CA94588
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Abstract

Last year we discussed the performance of a new parallel EELS spectrometer, the ENFINA. The spectrometer optics have been considerably improved over past designs and the detector changed from a photodiode to a charge coupled device that was designed specifically for spectroscopy. in this work we present application examples that demonstrate some of the capabilities of the ENFINA.

STEM spectrum imaging requires a spectrometer of high speed and sensitivity if useful data is to be collected in a short period of time. The ENFINA spectrometer achieves both of these through a radically improved point spread function, increased sensitivity, and fast detector readout. Useful spectrum images can be acquired in a few minutes. Figure 1 shows a dark-field STEM image of a typical semiconductor. A spectrum image containing 190 x 150 spectra was acquired from within the marked area.

Type
EELS Microanalysis at High Sensitivity: Advances in Spectrum Imaging, Energy Filtering and Detection (Organized by R. Leapman and J. Bruley)
Copyright
Copyright © Microscopy Society of America 2001

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References

References:

aBrink, H. A. et al, Proceedings of Microscopy and Microanalysis 2000, 212213 (2000)CrossRefGoogle Scholar