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Strain induced hardening and softening behaviors of deformed Cu and Cu–Ge alloys

Published online by Cambridge University Press:  24 February 2016

Y.L. Gong
Affiliation:
Faculty of Science, Kunming University of Science and Technology, Kunming 650093, Yunan Province, China
H.S. Kim
Affiliation:
Department of Materials Science and Engineering, Pohang University of Science and Technology, Pohang 790-784, South Korea
S.Y. Ren
Affiliation:
Ningbo Powerway Alloy Material Co., Ltd, Ningbo 315135, Zhejiang Province, China
S.D. Zeng
Affiliation:
Department of Thermal Engineering, Yunnan Institute of Measuring and Testing Technology, Kunming 650228, Yunan Province, China
X.K. Zhu*
Affiliation:
Faculty of Materials Science and Engineering, Kunming University of Science and Technology, Kunming 650093, Yunan Province, China
*
a) Address all correspondence to this author. e-mail: xk_zhu@hotmail.com
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Abstract

Herein, Cu and Cu–Ge alloys with different stacking fault energies (SFEs) are prepared via rolling at room temperature (RTR) and via a combination of high-pressure torsion (HPT) and RTR (HPT + RTR). The x-ray diffraction measurements reveal that the grain size, dislocation density, and twin density vary with the strain and SFEs. The tensile tests indicate that the strength of materials with medium SFEs increases initially and then slightly declines, while the ductility is enhanced by increasing the strain via HPT. In contrast, for low-SFE materials, enhanced strength and improved ductility may be achieved simultaneously through increasing the strain to a high level. The variation of strength with respect to strain is primarily dependent on the solute concentration and SFE. The underlying mechanisms governing the effect of strain and SFE on the microstructures and mechanical properties of the metals are also discussed.

Type
Articles
Copyright
Copyright © Materials Research Society 2016 

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References

REFERENCES

Valiev, R.Z. and Alexandrov, I.V.: Nanostructured materials from severe plastic deformation. Nanostruct. Mater. 12, 35 (1999).Google Scholar
Zhilyaev, A.P., Lee, S., Nurislamova, G.V., Valiev, R.Z., and Langdon, T.G.: Microhardness and microstructural evolution in pure nickel during high-pressure torsion. Scr. Mater. 44, 2753 (2001).Google Scholar
Segal, V.M.: Materials processing by simple shear. Mater. Sci. Eng., A 197, 157 (1995).Google Scholar
Stráská, J., Janeček, M., Gubicza, J., Krajňák, T., Yoon, E.Y., and Kim, H.S.: Evolution of microstructure and hardness in AZ31 alloy processed by high pressure torsion. Mater. Sci. Eng., A 625, 98 (2015).Google Scholar
Wongsa-Ngam, J., Kawasaki, M., and Langdon, T.: A comparison of microstructures and mechanical properties in a Cu–Zr alloy processed using different SPD techniques. J. Mater. Sci. 48, 4653 (2013).Google Scholar
Bazarnik, P., Huang, Y., Lewandowska, M., and Langdon, T.G.: Structural impact on the Hall–Petch relationship in an Al–5Mg alloy processed by high-pressure torsion. Mater. Sci. Eng., A 626, 9 (2015).Google Scholar
Xu, C., Horita, Z., and Langdon, T.G.: The evolution of homogeneity in processing by high-pressure torsion. Acta Mater. 55, 203 (2007).Google Scholar
Akbaripanah, F., Fereshteh-Saniee, F., Mahmudi, R., and Kim, H.K.: Microstructural homogeneity, texture, tensile and shear behavior of AM60 magnesium alloy produced by extrusion and equal channel angular pressing. Mater. Des. 43, 31 (2013).Google Scholar
Kawasaki, M., Ahn, B., and Langdon, T.G.: Significance of strain reversals in a two-phase alloy processed by high-pressure torsion. Mater. Sci. Eng., A 527, 7008 (2010).Google Scholar
Cho, T-S., Lee, H-J., Ahn, B., Kawasaki, M., and Langdon, T.G.: Microstructural evolution and mechanical properties in a Zn–Al eutectoid alloy processed by high-pressure torsion. Acta Mater. 72, 67 (2014).Google Scholar
Zhao, Y.H., Horita, Z., Langdon, T.G., and Zhu, Y.T.: Evolution of defect structures during cold rolling of ultrafine-grained Cu and Cu–Zn alloys: Influence of stacking fault energy. Mater. Sci. Eng., A 474, 342 (2008).CrossRefGoogle Scholar
Kawasaki, M.: Different models of hardness evolution in ultrafine-grained materials processed by high-pressure torsion. J. Mater. Sci. 49, 18 (2014).Google Scholar
Tian, Y.Z., Li, J.J., Zhang, P., Wu, S.D., Zhang, Z.F., Kawasaki, M., and Langdon, T.G.: Microstructures, strengthening mechanisms and fracture behavior of Cu–Ag alloys processed by high-pressure torsion. Acta Mater. 60, 269 (2012).Google Scholar
Harai, Y., Ito, Y., and Horita, Z.: High-pressure torsion using ring specimens. Scr. Mater. 58, 469 (2008).Google Scholar
Zhilyaev, A.P., Oh-ishi, K., Langdon, T.G., and McNelley, T.R.: Microstructural evolution in commercial purity aluminum during high-pressure torsion. Mater. Sci. Eng., A 410–411, 277 (2005).Google Scholar
Edalati, K., Horita, Z., Furuta, T., and Kuramoto, S.: Dynamic recrystallization and recovery during high-pressure torsion: Experimental evidence by torque measurement using ring specimens. Mater. Sci. Eng., A 559, 506 (2013).Google Scholar
Balasundar, I., Ravi, K.R., and Raghu, T.: Strain softening in oxygen free high conductivity (OFHC) copper subjected to repetitive upsetting-extrusion (RUE) process. Mater. Sci. Eng., A 583, 114 (2013).Google Scholar
Almazrouee, A.I., Al-Fadhalah, K.J., Alhajeri, S.N., and Langdon, T.G.: Microstructure and microhardness of OFHC copper processed by high-pressure torsion. Mater. Sci. Eng., A 641, 21 (2015).Google Scholar
Astafurova, E.G., Tukeeva, M.S., Maier, G.G., Melnikov, E.V., and Maier, H.J.: Microstructure and mechanical response of single-crystalline high-manganese austenitic steels under high-pressure torsion: The effect of stacking-fault energy. Mater. Sci. Eng., A 604, 166 (2014).Google Scholar
Balogh, L., Ungár, T., Zhao, Y., Zhu, Y.T., Horita, Z., Xu, C., and Langdon, T.G.: Influence of stacking-fault energy on microstructural characteristics of ultrafine-grain copper and copper-zinc alloys. Acta Mater. 56, 809 (2008).Google Scholar
Zhao, Y.H., Zhu, Y.T., Liao, X.Z., Horita, Z., and Langdon, T.G.: Tailoring stacking fault energy for high ductility and high strength in ultrafine grained Cu and its alloy. Appl. Phys. Lett. 89, 121906 (2006).Google Scholar
Zhang, Z.J., Duan, Q.Q., An, X.H., Wu, S.D., Yang, G., and Zhang, Z.F.: Microstructure and mechanical properties of Cu and Cu–Zn alloys produced by equal channel angular pressing. Mater. Sci. Eng., A 528, 4259 (2011).Google Scholar
Bahmanpour, H., Kauffmann, A., Khoshkhoo, M.S., Youssef, K.M., Mula, S., Freudenberger, J., Eckert, J., Scattergood, R.O., and Koch, C.C.: Effect of stacking fault energy on deformation behavior of cryo-rolled copper and copper alloys. Mater. Sci. Eng., A 529, 230 (2011).Google Scholar
Vinogradov, A., Merson, D.L., Patlan, V., and Hashimoto, S.: Effect of solid solution hardening and stacking fault energy on plastic flow and acoustic emission in Cu–Ge alloys. Mater. Sci. Eng., A 341, 57 (2003).Google Scholar
Gallagher, P.C.J.: The influence of alloying, temperature, and realted effects on the stacking fault energy. Metall. Trans. 1, 2429 (1970).Google Scholar
Koch, C.C., Morris, D.G., Lu, K., and Inoue, A.: Ductility of nanostructured materials. MRS Bull. 24, 54 (1999).Google Scholar
Ungár, T.: Characterization of nanocrystalline materials by X-ray line profile analysis. J. Mater. Sci. 42, 1584 (2007).Google Scholar
Zhao, Y.H., Liao, X.Z., Jin, Z., Valiev, R.Z., and Zhu, Y.T.: Microstructures and mechanical properties of ultrafine grained 7075 Al alloy processed by ECAP and their evolutions during annealing. Acta Mater. 52, 4589 (2004).Google Scholar
Williamson, G.K. and Smallman, R.E.: Dislocation densities in some annealed and cold-worked metals from measurements on the X-ray debye-scherrer spectrum. Philos. Mag. 1, 34 (1956).Google Scholar
Wagner, C.N.J.: Stacking faults by low-temperature cold work in copper and alpha brass. Acta Metall. 5, 427 (1957).CrossRefGoogle Scholar
Ungár, T.: Microstructural parameters from X-ray diffraction peak broadening. Scr. Mater. 51, 777 (2004).Google Scholar
Meyers, M.A., Vöhringer, O., and Lubarda, V.A.: The onset of twinning in metals: A constitutive description. Acta Mater. 49, 4025 (2001).Google Scholar
Xiao, G.H., Tao, N.R., and Lu, K.: Effects of strain, strain rate and temperature on deformation twinning in a Cu–Zn alloy. Scr. Mater. 59, 975 (2008).Google Scholar
Zhilyaev, A.P., Nurislamova, G.V., Kim, B.K., Baró, M.D., Szpunar, J.A., and Langdon, T.G.: Experimental parameters influencing grain refinement and microstructural evolution during high-pressure torsion. Acta Mater. 51, 753 (2003).Google Scholar
Edalati, K., Akama, D., Nishio, A., Lee, S., Yonenaga, Y., Cubero-Sesin, J.M., and Horita, Z.: Influence of dislocation–solute atom interactions and stacking fault energy on grain size of single-phase alloys after severe plastic deformation using high-pressure torsion. Acta Mater. 69, 68 (2014).Google Scholar
Li, Y., Zhao, Y.H., Liu, W., Xu, C., Horita, Z., Liao, X.Z., Zhu, Y.T., Langdon, T.G., and Lavernia, E.J.: Influence of grain size on the density of deformation twins in Cu–30%Zn alloy. Mater. Sci. Eng., A 527, 3942 (2010).Google Scholar
Tao, N.R. and Lu, K.: Nanoscale structural refinement via deformation twinning in face-centered cubic metals. Scr. Mater. 60, 1039 (2009).Google Scholar
Sun, P-L., Zhao, Y.H., Cooley, J.C., Kassner, M.E., Horita, Z., Langdon, T.G., Lavernia, E.J., and Zhu, Y.T.: Effect of stacking fault energy on strength and ductility of nanostructured alloys: An evaluation with minimum solution hardening. Mater. Sci. Eng., A 525, 83 (2009).Google Scholar
Zhao, Y-H., Bingert, J.F., Liao, X-Z., Cui, B-Z., Han, K., Sergueeva, A.V., Mukherjee, A.K., Valiev, R.Z., Langdon, T.G., and Zhu, Y.T.: Simultaneously increasing the ductility and strength of ultra-fine-grained pure copper. Adv. Mater. 18, 2949 (2006).Google Scholar