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Rapidly quenched Bi-containing high Tc superconducting oxide compositions

Published online by Cambridge University Press:  31 January 2011

K. Nassau ,
A. E. Miller ,
E. M. Gyorgy  and
T. Siegrist
K. Nassau
Affiliation:
AT & T Bell Laboratories, Murray Hill, New Jersey 07974
A. E. Miller
Affiliation:
AT & T Bell Laboratories, Murray Hill, New Jersey 07974
E. M. Gyorgy
Affiliation:
AT & T Bell Laboratories, Murray Hill, New Jersey 07974
T. Siegrist
Affiliation:
AT & T Bell Laboratories, Murray Hill, New Jersey 07974
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Abstract

Twin roller quenching from the melt at cooling rates of ∼107 K s−1 was used on several Bi-containing high Tc compositions. Pure glass was obtained in most compositions and the route of crystallization was studied by differential thermal and thermogravimetric analysis, x-ray diffraction, and magnetic measurements. Heating of the glasses produced poorly crystallized short-range-order-only as determined by x-ray diffraction, despite passing through several exotherms, some of which were very strong. This anomalous behavior deserves further investigation. On heating to higher temperatures the expected double-copper-oxide-layer high Tc phase formed sluggishly via intermediate CuBi2O4 and/or single-copper-oxide-layer Bi2(Sr, Cu)2CuO4 phases. Considerable oxygen absorption of about 0.5 O per Cu occurs during these steps, peaking at about 680 °C; some of this oxygen is lost again by the time the high Tc phase forms just below the melting point.

Type
Articles
Information
Journal of Materials Research , Volume 4 , Issue 6 , December 1989 , pp. 1330 - 1338
Copyright
Copyright © Materials Research Society 1989

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