Hostname: page-component-76fb5796d-zzh7m Total loading time: 0 Render date: 2024-04-25T09:37:21.176Z Has data issue: false hasContentIssue false

Pyrocarbon anisotropy as measured by electron diffraction and polarized light

Published online by Cambridge University Press:  31 January 2011

Xavier Bourrat
Affiliation:
Laboratoire des Composites Thermosructuraux (UMR 5801 CNRS-SNECMA-CEA-UB1), Université Bordeaux 1, 3 Allée La Boétie, F-33 600 Pessac, France
Béatrice Trouvat
Affiliation:
Laboratoire des Composites Thermosructuraux (UMR 5801 CNRS-SNECMA-CEA-UB1), Université Bordeaux 1, 3 Allée La Boétie, F-33 600 Pessac, France
Guillaume Limousin
Affiliation:
Laboratoire des Composites Thermosructuraux (UMR 5801 CNRS-SNECMA-CEA-UB1), Université Bordeaux 1, 3 Allée La Boétie, F-33 600 Pessac, France
Gérard Vignoles
Affiliation:
Laboratoire des Composites Thermosructuraux (UMR 5801 CNRS-SNECMA-CEA-UB1), Université Bordeaux 1, 3 Allée La Boétie, F-33 600 Pessac, France
François Doux
Affiliation:
SNECMA, BP 37, F-33 165 Saint Médard-en-Jalles cedex, France
Get access

Extract

This work deals with the measurement of pyrocarbon anisotropy on very thin fiber coatings used to control the interfacial behavior in carbon/carbon composites. Differentiation of the various pyrocarbons was performed through computerized image analysis of the electron diffraction patterns by measuring the azimuth opening of the carbon 002 diffraction arcs. This orientation angle decreases when the texture switches from rough to smooth laminar. The relationship with the polarized light measurement technique at a lower resolution is discussed.

Type
Articles
Copyright
Copyright © Materials Research Society 2000

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1.Ruland, W., Appl. Polymer Symp. 9, 293 (1969).Google Scholar
2.Trouvat, B., Bourrat, X., and Naslain, R., Proc. 23rd Biennial Conf. on Carbon, Pennstate 18–23 July 1997 (American Carbon Society, Washington, DC, 1997).Google Scholar
3.Trouvat, B., Thesis, University of Bordeaux 1, OA, 1635 (16 December 1996).Google Scholar
4.Bourrat, X., in Sciences of Carbon Materials, edited by Marsh, H. and Rodriguez-Reinosso, F. (Univ. Alicantes Publisher, Alicante, Spain 1999), Chap. 1.Google Scholar
5.Fiscbach, D.B., J. Appl. Phys. 37, 2202 (1966).CrossRefGoogle Scholar
6.Ruland, W., J. Appl. Phys. 38, 3585 (1967).CrossRefGoogle Scholar
7.Bacon, G.E., J. Appl. Chem. 6, 477 (1956).CrossRefGoogle Scholar
8.Diefendorf, R.J. and Tokarsky, E.W., Air Force Report AF 33(615)-70-C-1530 (1971).Google Scholar
9.Stevens, D.W., Proc. 6th Int. Materials Symposium, Univ. of California at Berkeley, 1976, pp. 129141.Google Scholar
10.Koizlik, K. and Grübmeier, H.B., Leitz-Mitt. Wiss. U. Techn. Bd. VI, No. 4 (1974), pp. 121126.Google Scholar
11.Hirai, T. and Yajima, S., J. Mater. Sci. 2, 18 (1967).CrossRefGoogle Scholar
12.Dupel, P., Bourrat, X., and Pailler, R., Carbon 33, 1193 (1995).CrossRefGoogle Scholar
13.Bourrat, X., Paillet, R., and Hanusse, P., Proc. of the 21st Biennial Conf. on Carbon, Buffalo, June 13–18, 1993, State Univ. of NY at Buffalo (Am. Carbon Society, Washington, DC, 1993), pp. 9495.Google Scholar
14.Naslain, R., in High Temperature Ceramic-Matrix-Composites, Ceramic Transactions. Vol. 58, edited by Evans, A.G. and Naslain, R. (1992), pp. 2339.Google Scholar
15.Jacques, S., Guette, A., Langlais, F., and Bourrat, X., J. Mater. Sci. 32, 2969 (1997).CrossRefGoogle Scholar
16.Ramdhor, P., Arch. Eisenhüttenwes Dtsch 25A (1928);Google Scholar
Schneiderhohn, H. and Ramdhor, P., in Lehrbuch der Erzmikroskopie (Berlin, 1941), T11.Google Scholar
17.Capdecome, L., Bull. Soc. Fr. Mineral. 78, 181 (1943).Google Scholar
18.McCartney, and Ergun, S., Fuel 37, 272 (1960);Google Scholar
Ergun, S., Nature 14, 135 (1967).CrossRefGoogle Scholar
19.Forest, R.A., Forest, H., Marsh, H., Cornford, C. and Kelly, B. T., in Chemistry and Physics of Carbon, edited by Thrower, P.L. (Marcel Dekker, New York, 1984), Vol. 19.Google Scholar
20.Rouzaud, J.N. and Oberlin, A., Thin Solids Films 105, 75 (1983).CrossRefGoogle Scholar
21.Bokros, J.C., in Chemistry and Physics of Carbon, edited by Walker, P.L. Jr., (Marcel Dekker, New York, 1969), Vol. 5, p. 1.Google Scholar
22.Warren, B.E., Phys. Rev. 59, 693 (1941).CrossRefGoogle Scholar
23.Oberlin, A., Carbon 17, 77 (1979).CrossRefGoogle Scholar