Hostname: page-component-848d4c4894-xfwgj Total loading time: 0 Render date: 2024-06-25T21:28:32.726Z Has data issue: false hasContentIssue false

Microwave-assisted synthesis of one-dimensional nanostructures

Published online by Cambridge University Press:  03 March 2011

Qingyi Lu
Affiliation:
Materials Research Institute, The Pennsylvania State University, University Park, Pennsylvania, 16802
Feng Gao
Affiliation:
Materials Research Institute, The Pennsylvania State University, University Park, Pennsylvania, 16802
Sridhar Komarneni*
Affiliation:
Materials Research Institute, The Pennsylvania State University, University Park, Pennsylvania, 16802
*
a)Address all correspondence to this author.e-mail: komarneni@psu.edu
Get access

Abstract

A microwave-assisted solvothermal method was used for the synthesis of selenium nanorods. The obtained selenium nanorods have axis ratios higher than 100 with their diameters in the range of 30–150 nm. This method is quite simple, rapid, adjustable, and general. Besides the effects of the experimental parameters on the synthesis of the selenium nanorods, the generality of this method has also been investigated, by which other one-dimensional nanostructures, metal lead and semiconductor cadmium sulfide nanorods, were also successfully synthesized.

Type
Articles
Copyright
Copyright © Materials Research Society 2004

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1Haram, S.K., Quinn, B.M., and Bard, A.J.: J. Am. Chem. Soc. 123, 8860 (2001).CrossRefGoogle Scholar
2Yu, H., Gibbons, P.C., Kelton, K.F., and E, W.: J. Am. Chem. Soc. 123, 9198 (2001).CrossRefGoogle Scholar
3Pileni, M.P.: J. Phys. Chem. B 105 3358 (2001).CrossRefGoogle Scholar
4Maoz, R., Frydman, E., Cohen, S.R., and J. Sagiv: Adv. Mater. 12, 424 (2000).3.0.CO;2-S>CrossRefGoogle Scholar
5Pan, Z.Y., Liu, X.J., Zhang, S.Y., Shen, G.J., Zhang, L.G., Lu, Z.H., and Liu, J.Z.: J. Phys. Chem. B 101, 9703 (1997).CrossRefGoogle Scholar
6Vossmeyer, T., DeIonno, E., and Heath, J.R.: Angew. Chem. Int. Ed. Engl. 36, 1080 (1997).CrossRefGoogle Scholar
7Xu, D., Xu, Y., D. Chen, Guo, G., Gui, L., and Tang, Y.: Adv. Mater. 12, 520 (2000).3.0.CO;2-#>CrossRefGoogle Scholar
8Song, J.H., Messer, B., Y. Wu, Kind, H., and Yang, P.: J. Am. Chem. Soc. 123, 9714 (2001).CrossRefGoogle Scholar
9Zhang, Z., Gekhtman, D., Dresselhaus, M.S., and Ying, J.Y.: Chem. Mater. 11, 1659 (1999).CrossRefGoogle Scholar
10Chen, C.C., Chao, C.Y., and Lang, Z.H.: Chem. Mater. 12, 1519 (2000).Google Scholar
11Hana, N.R., Gearheart, L., and Murphy, C.J.: J. Phys. Chem. B 105, 4065 (2001).Google Scholar
12Huang, M.H., Mao, S., H. Feick, Yan, H., Wu, Y., Kind, H., E. Weber, Russo, R., and Yang, P.: Science 292, 1897 (2001).CrossRefGoogle Scholar
13Mbindyo, J.K.N., Reiss, B.D., Martin, B.R., Keating, C.D., Natan, M.J., and Mallouk, T.E.: Adv. Mater. 13, 249 (2001).3.0.CO;2-9>CrossRefGoogle Scholar
14Peng, X., Manna, L., Yang, W., Wickham, J., Scher, E., Kadavanich, A., and Alivisatos, A.P.: Nature 404, 59 (2000).CrossRefGoogle Scholar
15Hatzor, A. and Weiss, P.S.: Science 291, 1019 (2001).Google Scholar
16Wang, Z.L., Gao, R.P., Gole, J.L., and Stout, J.D.: Adv. Mater. 12, 1938 (2000).3.0.CO;2-4>CrossRefGoogle Scholar
17Wanger, R.S. and Ellis, W.C.: Appl. Phys. Lett. 4, 89 (1964).Google Scholar
18Hu, J.T., Odom, T.W., and Lieber, C.M.: Acc. Chem. Res. 32, 435 (1999).CrossRefGoogle Scholar
19Wu, Y. and Yang, P.: J. Am. Chem. Soc. 123, 3165 (2001).CrossRefGoogle Scholar
20Trentler, T. J., Hickman, K.M., Goel, C., Viano, A.M., Gibbons, P.C., and Buhro, W.E.: Science 270, 1791 (1995).CrossRefGoogle Scholar
21Masuda, H., Yanagishita, T., Yasui, K., Nishio, K., Yagi, I., Rao, T.N., and Fujishima, A.: Adv. Mater. 13, 247 (2001).3.0.CO;2-H>CrossRefGoogle Scholar
22Routkevitch, D., Bigioni, T., Moskovits, M., and Xu, J.M.: J. Phys. Chem. 100, 14037 (1996).CrossRefGoogle Scholar
23Han, W., Fan, S., and Li, Q.: Appl. Phys. Lett. 71, 2271 (1997).CrossRefGoogle Scholar
24Han, W., Fan, S., Li, Q.: Science 277, 1287 (1997).CrossRefGoogle Scholar
25Parala, H., Winkler, H., Kolbe, M., Wohlfart, A., Fischer, R.A., Schmechel, R., and Seggern, H.V.: Adv. Mater. 12, 1050 (2000).3.0.CO;2-T>CrossRefGoogle Scholar
26Chomski, E., Dag, O., Kuperman, A., Coombs, N., and Ozin, G.A.: Chem. Vap. Deposition 2, 8 (1996).CrossRefGoogle Scholar
27Aronson, B.J., Blanford, C.F., and Stein, A.: Chem. Mater. 9, 2842 (1997).CrossRefGoogle Scholar
28Hirai, T., Okubo, H., and Komasawa, I.: J. Phys. Chem. B 103, 4228 (1999).CrossRefGoogle Scholar
29Han, Y.J., Kim, J.M., and Stucky, G.D.: Chem. Mater. 12, 2068 (2000).CrossRefGoogle Scholar
30Gao, F., Lu, Q., Liu, X., Yan, Y., and Zhao, D.: Nano Lett. 1, 743 (2001).CrossRefGoogle Scholar
31Li, M., Schnablegger, H., Mann, S.: Nature 402, 393 (1999).CrossRefGoogle Scholar
32Shi, H., Qi, L., Ma, J., and Cheng, H.: J. Am. Chem. Soc. 125, 3450 (2003).CrossRefGoogle Scholar
33Li, X.L., Liu, J.F., and Li, Y.D.: Inorg. Chem. 42, 921 (2003).CrossRefGoogle Scholar
34Lee, K., Seo, W.S., and Park, J.T.: J. Am. Chem. Soc. 125, 3408 (2003).CrossRefGoogle Scholar
35Xiong, Y., Xie, Y., Li, Z., and Wu, C.: Chem. Eur. J. 9, 1645 (2003).CrossRefGoogle Scholar
36Patzke, G.R., Krumeich, F., and Nesper, R.: Angew. Chem. Int. Ed. Engl. 41, 2447 (2002).3.0.CO;2-K>CrossRefGoogle Scholar
37Tang, K.B., Qian, Y.T., Zeng, J.H., and Yang, X.G.: Adv. Mater. 15, 448 (2003).CrossRefGoogle Scholar
38Manna, L., Scher, E.C., and Alivisatos, A.P.: J. Am. Chem. Soc. 122, 12700 (2000).CrossRefGoogle Scholar
39Wang, H., Zhang, J.R., and Zhu, J.J.: J. Cryst. Growth 233, 829 (2001).CrossRefGoogle Scholar
40Liao, X.H., Chen, N.Y., Xu, S., Yang, S.B., and Zhu, J.J.: J. Cryst. Growth 252, 593 (2003).CrossRefGoogle Scholar
41Komarneni, S., Roy, R., and Li, Q.H.: Mater. Res. Bull. 27, 1393 (1992).CrossRefGoogle Scholar
42Murugan, A.V., Sonawane, R.S., Kale, B.B., Apte, S.K., and Kulkarni, A.V.: Mater. Chem. Phys. 71, 98 (2001).CrossRefGoogle Scholar
43Komarneni, S., Li, D., Newalkar, B., Katsuki, H., and Bhalla, A.S.: Langmuir 18, 5959 (2002).CrossRefGoogle Scholar
44Arafat, A., Jansen, J.C., Ebaid, A.R., Bekkum, H.V.: Zeolites 13, 162 (1993).CrossRefGoogle Scholar
45Wu, C.G. and Bein, T.: Chem. Commun. 925 (1996).CrossRefGoogle Scholar
46Hicks, R. and Majetich, G.: J. Microwave Power Electromagn. Eng. 30, 27 (1995).Google Scholar
47Abramovitch, R.A.: Org. Prep. Proc. Int. 23, 283 (1991).CrossRefGoogle Scholar
48Gedye, R.N., Rank, W., and Westaway, K.C.: Can. J. Chem. 69, 706 (1991).CrossRefGoogle Scholar
49Bond, G., Moyes, R.S., and Whan, D.A.: Catal. Today 17, 429 (1993).Google Scholar
50Yuji, W., Hiromitsu, K., Takao, S., Hirotaro, M., Takayuki, S., Takayuki, K., and Shozo, Y.: Chem. Lett. 607 (1999).Google Scholar
51Gallis, K.W. and Landry, C.C.: Adv. Mater. 13, 23 (2001).3.0.CO;2-9>CrossRefGoogle Scholar
52Boxall, D.L. and Lukehart, C.M.: Chem. Mater. 13, 806 (2001).CrossRefGoogle Scholar
53Palchik, O., Zhu, J.J., and Gedanken, A.: J. Mater. Chem. 10, 1251 (2000).CrossRefGoogle Scholar
54Palchik, O., Avivi, S., Pinkert, D., and Gedanken, A.: Nanostruct. Mater. 11, 41 (1999).CrossRefGoogle Scholar
55Tu, W. and Liu, H: J. Mater. Chem. 10, 2207 (2000).CrossRefGoogle Scholar
56He, J., Zhao, X.N., Zhu, J.J., and Wang, J.: J. Cryst. Growth 240, 389 (2002).CrossRefGoogle Scholar
57Zhu, J.J., Wang, H., Zhu, J.M., and Wang, J.: Mater. Sci. Eng. B-Solid 94, 136 (2002).CrossRefGoogle Scholar
58Zhu, J.J., Palchik, O., Chen, S., and Gedanken, A.: J. Phys. Chem. B 104, 7344 (2000).CrossRefGoogle Scholar
59Wu, H.Q., Shao, M.W., Gu, J.S., and Wei, X.W.: Chin. J. Inorg. Chem. 19, 107 (2003).Google Scholar
60Tao, X.C. and Shao, M.W.: Chin. J. Chem. 20, 1121, 2002.CrossRefGoogle Scholar
61Liao, X.H., Wang, H., Zhu, J.J., and Chen, H.Y.: Mater. Res. Bull. 36, 2339 (2001).CrossRefGoogle Scholar
62Liao, X.H., Zhu, J.M., Zhu, J.J., Xu, J.Z., and Chen, H.Y.: Chem. Commun. 937 (2001).CrossRefGoogle Scholar
63Gao, X., Gao, T., and Zhang, L.: J. Mater. Chem. 13, 6 (2003).CrossRefGoogle Scholar
64Gates, B., Mayers, B., Grossman, A., and Xia, Y.: Adv. Mater. 14, 1749 (2002).3.0.CO;2-Z>CrossRefGoogle Scholar
65Zhang, X., Xie, Y., Xu, F., Liu, X., Zhang, S., and Tian, X.: Solid State Sci. 5, 525 (2003).CrossRefGoogle Scholar
66Cheng, B. and Samulski, E.T.: Chem. Commum. 2024 (2003).CrossRefGoogle Scholar
67Li, Y., Liao, H., Ding, Y., Qian, Y., Yang, L., and Zhou, G: Chem. Mater. 10, 2301 (1998).CrossRefGoogle Scholar
68Yu, S.H., Wu, Y.S., Yang, J., Han, Z.H., Xie, Y., Qian, Y.T., and Liu, X.M.: Chem. Mater. 10, 2309 (1998).CrossRefGoogle Scholar
69Gao, F., Lu, Q., Xie, S., and Zhao, D.: Adv. Mater. 14, 1537 (2002).3.0.CO;2-Q>CrossRefGoogle Scholar