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This article presents a novel microscratch technique for the determination of the fracture toughness of materials from scratch data. While acoustic emission and optical imaging devices provide quantitative evidence of fracture processes during scratch tests, the technique proposed here provides a quantitative means to assess the fracture toughness from the recorded forces and depth of penetration. We apply the proposed method to a large range of materials, from soft (polymers) to hard (metal), spanning fracture toughness values over more than two orders of magnitude. The fracture toughness values so obtained are in excellent agreement with toughness values obtained for the same materials by conventional fracture tests. The fact that the proposed microscratch technique is highly reproducible, almost nondestructive, and requires only small material volumes makes this technique a powerful tool for the assessment of fracture properties for microscale materials science and engineering applications.
Hide All1.Anunmana, C., Anusavice, K.J., and Mecholsky, J.J. Jr.: Residual stress in glass: Indentation crack and fractography approaches. Dent. Mater. 25, 1453 (2009).2.Harding, D.S., Oliver, W.C., and Pharr, G.M.: Cracking during nano indentation and its use in the measurement of fracture toughness. Mater. Res. Soc. Symp. Proc. 356, 663 (1995).3.Quinn, G.D. and Bradt, R.C.: On the Vickers indentation fracture toughness test. J. Am. Ceram. Soc. 90, 673 (2007).4.Widjaja, S., Yip, T.H., and Limarga, A.M.: Measurement of creep-induced localized residual stress in soda-lime glass using nano-indentation technique. Mater. Sci. Eng., A 318, 211 (2001).5.ASTM C1624-05, Standard Test Method for Adhesion Strength and Mechanical Failure Modes of Ceramic Coatings by Quantitative Single Point Scratch Testing.6.Ollendorf, H. and Schneider, D.: A comparative study of adhesion test methods for hard coatings. Surf. Coat. Technol. 113, 86 (1999).7.Wredenberg, F. and Larsson, P.L.: Scratch testing of metals and polymers: Experiments and numerics. Wear 266, 76 (2009).8.ASTM G-171 03, Standard Test Method for Scratch Hardness of Materials Using a Diamond Stylus.9.Bard, R. and Ulm, F-J.: Scratch hardness strength solutions for cohesive–frictional materials. Int. J. Numer. Anal. Methods Geomech. (2010)., doi: 10.1002/nag.1008.10.Barenblatt, G.I.: The mathematical theory of equilibrium cracks in brittle fracture. Adv. Appl. Mech. 7, 55 (1962).11.Akono, A-T., Reis, P.M., and Ulm, F-J.: Scratching as a fracture process: From butter to steel. Phys. Rev. Lett. 106, 204302 (2011).12.Akono, A-T. and Ulm, F-J.: Fracture scaling relations for scratch tests of axisymmetric shape. J. Mech. Phys. Solids (2012). In press.13.Miller, M., Bobko, C., Vandamme, M., and Ulm, F-J.: Surface roughness criteria for cement paste nanoindentation. Cem. Concr. Res. 38, 467 (2008).14.Randall, N.X., Favaro, G., and Frankel, C.H.: The effect of intrinsic parameters on the critical load as measured with the scratch test method. Surf. Coat. Technol. 137, 146 (2001).15.Briscoe, B.J., Fiori, L., and Pelillo, E.: Nano-indentation of polymeric surfaces. J. Phys. D: Appl. Phys. 31, 2395 (1998).16.VanLandingham, M.R., Juliano, T.F., and Hagon, M.J.: Measuring tip shape for instrumented indentation using atomic force microscopy. Meas. Sci. Technol. 16, 2173 (2005).17.Hertzberg, R.W., Skibo, M.D., and Manson, J.A.: Fatigue crack propagation in polyacetal. J. Mater. Sci. 13, 1038 (1978).18.Hill, A.J. and Agrawal, C.M.: Positron lifetime spectroscopy characterization of thermal history effects on polycarbonate. J. Mater. Sci. 25, 5036 (1990).19.Bauccio, M.L.: ASM Metals Reference Book, 3rd ed.ASM International, Materials Park, OH, 1993).20.Matthews, W.T.: Data Handbook for Metals (AMMRC MS73-6, U.S. Army Materials and Mechanics Research Center, Watertown, MA, 1973).21.Akono, A-T. and Ulm, F-J.: Scratch test model for the determination of fracture toughness. Eng. Fract. Mech. 78, 334 (2011).
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- ISSN: 0884-2914
- EISSN: 2044-5326
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