Hostname: page-component-8448b6f56d-m8qmq Total loading time: 0 Render date: 2024-04-23T12:40:32.326Z Has data issue: false hasContentIssue false

The effect of microstructure heterogeneity on the microscale deformation of ultrafine-grained aluminum

Published online by Cambridge University Press:  12 August 2014

Adam D. Kammers
Affiliation:
Department of Mechanical Engineering, The University of Michigan, Ann Arbor, Michigan 48109, USA
Jittraporn Wongsa-Ngam
Affiliation:
Department of Mechanical Engineering, Faculty of Engineering, King Mongkut's Institute of Technology Ladkrabang, Bangkok 10520, Thailand
Terence G. Langdon
Affiliation:
Departments of Aerospace & Mechanical Engineering and Materials Science, University of Southern California, Los Angeles, California 90089-1453, USA; and Materials Research Group, Faculty of Engineering and the Environment, University of Southampton, Southampton SO17 1BJ, United Kingdom
Samantha Daly*
Affiliation:
Department of Materials Science & Engineering, The University of Michigan, Ann Arbor, Michigan 48109, USA; and Department of Mechanical Engineering, The University of Michigan, Ann Arbor, Michigan 48109, USA
*
a)Address all correspondence to this author. e-mail: samdaly@umich.edu
Get access

Abstract

A combined approach of scanning electron microscopy and digital image correlation was used to examine microstructure-scale strain localization and active deformation mechanisms in ultrafine-grained (UFG) high purity (99.99%) aluminum processed by equal-channel angular pressing (ECAP). The results from tensile tests demonstrate a strong relationship between the heterogeneous microstructure and strain localization. The localized deformation was investigated in areas that contain significantly different microstructural features typical of ECAP processed aluminum. It was found that areas of the UFG microstructure containing primarily low angle grain boundaries deformed by dislocation slip and behaved similarly to a coarse-grained material. The greatest strain localization occurred at high angle grain boundaries (HAGBs) separating distinct microstructure regions and with median surface trace angles of approximately 26.6°. In areas of banded microstructure, shear strain localization as high as 30% and shear displacements of up to 500 nm occurred at the HAGBs separating bands, suggesting grain boundary sliding.

Type
Articles
Copyright
Copyright © Materials Research Society 2014 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

Valiev, R.Z., Estrin, Y., Horita, Z., Langdon, T.G., Zechetbauer, M.J., and Zhu, Y.T.: Producing bulk ultrafine-grained materials by severe plastic deformation. JOM 58(4), 33 (2006).CrossRefGoogle Scholar
Valiev, R.Z., Enikeev, N.A., Murashkin, M.Y., Kazykhanov, V.U., and Sauvage, X.: On the origin of the extremely high strength of ultrafine-grained Al alloys produced by severe plastic deformation. Scr. Mater. 63, 949 (2010).CrossRefGoogle Scholar
Valiev, R.Z. and Langdon, T.G.: Principles of equal-channel angular pressing as a processing tool for grain refinement. Prog. Mater. Sci. 51, 881 (2006).CrossRefGoogle Scholar
Valiev, R.Z., Alexandrov, I.V., Zhu, Y.T., and Lowe, T.C.: Paradox of strength and ductility in metals processed by severe plastic deformation. J. Mater. Res. 17, 5 (2002).CrossRefGoogle Scholar
Dvorak, J., Sklenicka, V., and Horita, Z.: Microstructural evolution and mechanical properties of high purity aluminium processed by equal-channel angular pressing. Mater. Trans. 49, 15 (2008).CrossRefGoogle Scholar
Estrin, Y. and Vinogradov, A.: Extreme grain refinement by severe plastic deformation: A wealth of challenging science. Acta Mater. 61, 782 (2013).CrossRefGoogle Scholar
Lowe, T.C.: Metals and alloys nanostructured by severe plastic deformation: Commercialization pathways. JOM 58(4), 28 (2006).CrossRefGoogle Scholar
Valiev, R.Z., Semenova, I.P., Latysh, V.V., Rack, H., Lowe, T.C., Petruzelka, J., Dluhos, L., Hrusak, D., and Sochova, J.: Nanostructured titanium for biomedical applications. Adv. Biomater. 10, B15 (2008).Google Scholar
Iwahashi, Y., Wang, J., Horita, Z., Nemoto, M., and Langdon, T.G.: Principle of equal-channel angular pressing for the processing of ultra-fine grained materials. Scr. Mater. 35, 143 (1996).CrossRefGoogle Scholar
Langdon, T.G.: The principles of grain refinement in equal-channel angular pressing. Mater. Sci. Eng., A 462, 3 (2007).CrossRefGoogle Scholar
Langdon, T.G.: Twenty-five years of ultrafine-grained materials: Achieving exceptional properties through grain refinement. Acta Mater. 61, 7035 (2013).CrossRefGoogle Scholar
Furukawa, M., Horita, Z., and Langdon, T.G.: Factors influencing the shearing patterns in equal-channel angular pressing. Mater. Sci. Eng., A 332, 97 (2002).CrossRefGoogle Scholar
Iwahashi, Y., Furukawa, M., Horita, Z., Nemoto, M., and Langdon, T.G.: Microstructural characteristics of ultrafine-grained aluminum produced using equal-channel angular pressing. Metall. Mater. Trans. A 29, 2245 (1998).CrossRefGoogle Scholar
Beyerlein, I.J. and Tóth, L.S.: Texture evolution in equal-channel angular extrusion. Prog. Mater. Sci. 54, 427 (2009).CrossRefGoogle Scholar
Terhune, S.D., Swisher, D.L., Oh-ishi, K., Horita, Z., Langdon, T.G., and McNelley, T.R.: An investigation of microstructure and grain-boundary evolution during ECA pressing of pure aluminum. Metall. Mater. Trans. A 33, 2173 (2002).CrossRefGoogle Scholar
Oh-ishi, K., Zhilyaev, A.P., and McNelley, T.R.: Effect of strain path on evolution of deformation bands during ECAP of pure aluminum. Mater. Sci. Eng., A 410411, 183 (2005).CrossRefGoogle Scholar
Zhilyaev, A.P., Swisher, D.L., Oh-ishi, K., Langdon, T.G., and McNelley, T.R.: Microtexture and microstructure evolution during processing of pure aluminum by repetitive ECAP. Mater. Sci. Eng., A 429, 137 (2006).CrossRefGoogle Scholar
Reihanian, M., Ebrahimi, R., Moshksar, M.M., Terada, D., and Tsuji, N.: Microstructure quantification and correlation with flow stress of ultrafine grained commercially pure Al fabricated by equal channel angular pressing (ECAP). Mater. Charact. 59, 1312 (2008).CrossRefGoogle Scholar
Li, S., Beyerlein, I.J., Alexander, D.J., and Vogel, S.C.: Texture evolution during equal channel angular extrusion: Effect of initial texture from experiment and simulation. Scr. Mater. 52, 1099 (2005).CrossRefGoogle Scholar
Zhu, Y.T. and Lowe, T.C.: Observations and issues on mechanisms of grain refinement during ECAP process. Mater. Sci. Eng., A 291, 46 (2000).CrossRefGoogle Scholar
Kawasaki, M., Horita, Z., and Langdon, T.G.: Microstructural evolution in high purity aluminum processed by ECAP. Mater. Sci. Eng., A 524, 143 (2009).CrossRefGoogle Scholar
Chinh, N.Q., Szommer, P., Horita, Z., and Langdon, T.G.: Experimental evidence for grain-boundary sliding in ultrafine-grained aluminum processed by severe plastic deformation. Adv. Mater. 18, 34 (2006).CrossRefGoogle Scholar
Chinh, N.Q., Szommer, P., Csanádi, T., and Langdon, T.G.: Flow processes at low temperatures in ultrafine-grained aluminum. Mater. Sci. Eng., A 434, 326 (2006).CrossRefGoogle Scholar
Chinh, N.Q., Győri, T., Valiev, R.Z., Szommer, P., Varga, G., Havancsák, K., and Langdon, T.G.: Observations of unique plastic behavior in micro-pillars of an ultrafine-grained alloy. MRS Commun. 2, 75 (2012).CrossRefGoogle Scholar
Sabirov, I., Barnett, M.R., Estrin, Y., Timokhina, I., and Hodgson, P.D.: Deformation mechanisms in an ultra-fine grained Al alloy. Int. J. Mater. Res. 100, 1679 (2009).CrossRefGoogle Scholar
Sabirov, I., Barnett, M.R., Estrin, Y., and Hodgson, P.D.: The effect of strain rate on the deformation mechanisms and the strain rate sensitivity of an ultra-fine-grained Al alloy. Scr. Mater. 61, 181 (2009).CrossRefGoogle Scholar
Sabirov, I., Estrin, Y., Barnett, M.R., Timokhina, I., and Hodgson, P.D.: Tensile deformation of an ultrafine-grained aluminium alloy: Micro shear banding and grain boundary sliding. Acta Mater. 56, 2223 (2008).CrossRefGoogle Scholar
Ivanov, K.V. and Naydenkin, E.V.: Grain boundary sliding in ultrafine-grained aluminum under tension at room temperature. Scr. Mater. 66, 511 (2012).CrossRefGoogle Scholar
May, J., Höppel, H.W., and Göken, M.: Strain rate sensitivity of ultrafine-grained aluminium processed by severe plastic deformation. Scr. Mater. 53, 189 (2005).CrossRefGoogle Scholar
Höppel, H.W., May, J., Eisenlohr, P., and Göken, M.: Strain rate sensitivity of ultrafine-grained materials. Z. Metallkd. 96, 566 (2005).CrossRefGoogle Scholar
Böhner, A., Maier, V., Durst, K., Höppel, H.W., and Göken, M.: Macro- and nanomechanical properties and strain rate sensitivity of accumulative roll bonded and equal channel angular pressed ultrafine-grained materials. Adv. Eng. Mater. 13, 251 (2011).CrossRefGoogle Scholar
Peters, W.H. and Ranson, W.F.: Digital imaging techniques in experimental stress analysis. Opt. Eng. 21, 427 (1982).CrossRefGoogle Scholar
Sutton, M.A., Wolters, W.J., Peters, W.H., Ranson, W.F., and McNeill, S.R.: Determination of displacements using an improved digital correlation method. Image Vision Comput. 1, 133 (1983).CrossRefGoogle Scholar
Sutton, M.A., Orteu, J-J., and Schreier, H.: Digital Image Correlation (DIC), in Image Correlation for Shape, Motion and Deformation Measurements (Springer US, Boston, MA, 2009), pp. 81116.Google Scholar
Ahn, B., Lavernia, E.J., and Nutt, S.R.: Dynamic observations of deformation in an ultrafine-grained Al–Mg alloy with bimodal grain structure. J. Mater. Sci. 43, 7403 (2008).CrossRefGoogle Scholar
Ahn, B. and Nutt, S.R.: Strain mapping of Al–Mg Alloy with multi-scale grain structure using digital image correlation method. Exp. Mech. 50, 117 (2010).CrossRefGoogle Scholar
Zhang, Y., Topping, T.D., Lavernia, E.J., and Nutt, S.R.: Dynamic micro-strain analysis of ultrafine-grained aluminum magnesium alloy using digital image correlation. Metall. Mater. Trans. A 45, 47 (2013).CrossRefGoogle Scholar
Nakashima, K., Horita, Z., Nemoto, M., and Langdon, T.G.: Development of a multi-pass facility for equal-channel angular pressing to high total strains. Mater. Sci. Eng., A 281, 82 (2000).CrossRefGoogle Scholar
Furukawa, M., Iwahashi, Y., Horita, Z., Nemoto, M., and Langdon, T.G.: The shearing characteristics associated with equal-channel angular pressing. Mater. Sci. Eng., A 257, 328 (1998).CrossRefGoogle Scholar
Oh-ishi, K., Horita, Z., Furukawa, M., Nemoto, M., and Langdon, T.G.: Optimizing the rotation conditions for grain refinement in equal-channel angular pressing. Metall. Mater. Trans. A 29, 2011 (1998).CrossRefGoogle Scholar
Kammers, A.D. and Daly, S.: Self-assembled nanoparticle surface patterning for improved digital image correlation in a scanning electron microscope. Exp. Mech. 53, 1333 (2013).CrossRefGoogle Scholar
Vic-2D [software]: Correlated Solutions Inc, Columbia, SC, 2009.Google Scholar
Kammers, A.D. and Daly, S.: Digital image correlation under scanning electron microscopy: Methodology and validation. Exp. Mech. 53, 1743 (2013).CrossRefGoogle Scholar
Sutton, M.A., Li, N., Joy, D.C., Reynolds, A.P., and Li, X.: Scanning electron microscopy for quantitative small and large deformation measurements Part I: SEM imaging at magnifications from 200 to 10,000. Exp. Mech. 47, 775 (2007).CrossRefGoogle Scholar
Sutton, M.A., Li, N., Garcia, D., Cornille, N., Orteu, J-J., McNeill, S.R., Schreier, H.W., Li, X., and Reynolds, A.P.: Scanning electron microscopy for quantitative small and large deformation measurements Part II: Experimental validation for magnifications from 200 to 10,000. Exp. Mech. 47, 789 (2007).CrossRefGoogle Scholar
Sutton, M.A., Li, N., Garcia, D., Cornille, N., Orteu, J-J., McNeill, S.R., Schreier, H.W., and Li, X.: Metrology in a scanning electron microscope: Theoretical developments and experimental validation. Meas. Sci. Technol. 17, 2613 (2006).CrossRefGoogle Scholar
Bornert, M., Brémand, F., Doumalin, P., Dupré, J-C., Fazzini, M., Grédiac, M., Hild, F., Mistou, S., Molimard, J., Orteu, J-J., Robert, L., Surrel, Y., Vacher, P., and Wattrisse, B.: Assessment of digital image correlation measurement errors: Methodology and results. Exp. Mech. 49, 353 (2009).CrossRefGoogle Scholar
Luster, J. and Morris, M.A.: Compatibility of deformation in two-phase Ti-Al alloys: Dependence on microstructure and orientation relationships. Metall. Mater. Trans. A 26, 1745 (1995).CrossRefGoogle Scholar
Bieler, T.R., Eisenlohr, P., Roters, F., Kumar, D., Mason, D.E., Crimp, M.A., and Raabe, D.: The role of heterogeneous deformation on damage nucleation at grain boundaries in single phase metals. Int. J. Plast. 25, 1655 (2009).CrossRefGoogle Scholar