Hostname: page-component-76fb5796d-wq484 Total loading time: 0 Render date: 2024-04-26T14:10:02.262Z Has data issue: false hasContentIssue false

Determination of the elastic properties of glasses and polymers exploiting the resonant characteristic of depth-sensing indentation tests

Published online by Cambridge University Press:  31 January 2011

D. Lorenz*
Affiliation:
Fachbereich Physik, Martin-Luther-University Halle-Wittenberg, F.-Bach-Platz 6, 06108 Halle, Germany
W. Fränzel
Affiliation:
Fachbereich Physik, Martin-Luther-University Halle-Wittenberg, F.-Bach-Platz 6, 06108 Halle, Germany
M. Einax
Affiliation:
Fachbereich Physik, Martin-Luther-University Halle-Wittenberg, F.-Bach-Platz 6, 06108 Halle, Germany
P. Grau*
Affiliation:
Fachbereich Physik, Martin-Luther-University Halle-Wittenberg, F.-Bach-Platz 6, 06108 Halle, Germany
G. Berg
Affiliation:
Fachbereich Physik, Martin-Luther-University Halle-Wittenberg, F.-Bach-Platz 6, 06108 Halle, Germany
Get access

Abstract

Depth-sensing indentation tests can be used to estimate the Young's modulus, hardness, and other characteristics of material behavior. For many materials, the unloading segment of the load–depth curve contains only elastic recovery while the loading segment can contain elastic and plastic deformation. In this paper a new method is presented to determine the Young's modulus of a material from the loading segment of an indentation test. A depth-sensitive hardness tester was used with a load cell integrated into the closed-loop system. Defined mechanical oscillations with constant frequency were generated by adding a piezoelectric stack to the closed loop of the hardness measurement system. Thus the resonance response of the system was obtained, which includes information regarding the stiffness of the tested material. This new method was tested on two polymers and two glasses, an optical and a conventional one. The results obtained for the Young's modulus were in good agreement with other accepted methods.

Type
Articles
Copyright
Copyright © Materials Research Society 2001

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1. European Technical norm ISO DIN 14577 (1999).Google Scholar
2.Fröhlich, F., Grau, P., and Grellmann, W., Phys. Status Solidi A 42, 79 (1977).CrossRefGoogle Scholar
3.Oliver, W.C. and Pharr, G.M., J. Mater. Res. 7, 1564 (1992).CrossRefGoogle Scholar
4.Grau, P., Meinhard, H., and Mosch, S., in Fundamentals of Nanoindentation and Nanotribology, edited by Moody, N.R., Gerberich, W.W., Burnham, N., and Baker, S.P. (Mater. Res. Soc. Symp. Proc. 522, Warrendale, PA, 1998), pp. 153158.Google Scholar
5.Pethica, J.B. and Oliver, W.C., in Thin Films: Stress and Mechani-cal Properties, edited by Bravman, J.C., Nix, W.D., Barnett, D.M., and Smith, D.A. (Mater. Res. Soc. Symp. Proc. 130, Pittsburgh, PA, 1989), p. 13.Google Scholar
6.Syed Asif, S.A. and Colton, R.J., Rev. Sci. Instr. 70, 2408 (1999).CrossRefGoogle Scholar
7.Lorenz, D., Fränzel, W., and Grau, P., German Patent DE 197 56 045 A1 (June 1999).Google Scholar
8.Sneddon, I.N., Int. J. Engng. Sci. 3, 47 (1965).CrossRefGoogle Scholar
9.Mencik, J. and Swain, M.V., Mater. Forum 18, 277 (1994).Google Scholar
10.Cheng, Y-T. and Cheng, Ch-M., in Fundamentals of Nanoindentation and Nanotribology, edited by Moody, N.R., Gerberich, W.W., Burnham, N., and Baker, S.P. (Mater. Res. Soc. Symp. Proc. 522, Warrendale, PA, 1998), pp. 139144.Google Scholar
11.Sargent, P.M., ASTM Special Technical Publication No. 889, edited by Blau, P.J. and Lawn, B.R. (American Society for Testing and Materials, Philadelphia, PA, 1986), pp. 160174.Google Scholar
12.Grau, P., Berg, G., Meinhard, H., and Mosch, S., J. Am. Ceram. Soc. 81, 1557 (1998).CrossRefGoogle Scholar
13.Nix, W.D., Mater. Sci. Eng. A 234–236, 37 (1997).CrossRefGoogle Scholar
14.Grau, P., Berg, G., and Fränzel, W., Glass Sci. Technol. 66, 313 (1993).Google Scholar
15.Grau, P., Berg, G., Fränzel, W., and Meinhard, H., Phys. Status Solidi A 146, 537 (1994).CrossRefGoogle Scholar
16.Grau, P., Berg, G., Oettel, H., and Wiedemann, R., Phys. Status Solidi A 159, 447 (1997).3.0.CO;2-G>CrossRefGoogle Scholar
17.Neideck, K., Fränzel, W., and Grau, P., J. Macromol. Sci.-Phys. B 38, 669 (1999).CrossRefGoogle Scholar