Hostname: page-component-77c89778f8-m8s7h Total loading time: 0 Render date: 2024-07-19T11:53:53.470Z Has data issue: false hasContentIssue false

A Study on the Microstructure of Preferred Orientation of Lead Zirconate Titanate (PZT) Thin Films

Published online by Cambridge University Press:  31 January 2011

Chang Jung Kim
Affiliation:
Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology, Kuseong Dong 373–1, Yusung Gu, Taejon, Korea
Dae Sung Yoon
Affiliation:
Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology, Kuseong Dong 373–1, Yusung Gu, Taejon, Korea
Joon Sung Lee
Affiliation:
Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology, Kuseong Dong 373–1, Yusung Gu, Taejon, Korea
Chaun Gi Choi
Affiliation:
Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology, Kuseong Dong 373–1, Yusung Gu, Taejon, Korea
Kwangsoo No
Affiliation:
Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology, Kuseong Dong 373–1, Yusung Gu, Taejon, Korea
Get access

Abstract

The lead zirconate titanate (PZT) thin films were fabricated using sol-gel spin coating onto Pt/Ti/glass substrates. Effects of the holding time for pyrolysis and the coating cycle on the preferred orientation of the PZT thin films were studied. The films were fabricated with different coating cycles (3, 5, 7, 9, 11), dried at 330 °C for different holding times (5, 30, 60 min), and then annealed at the same temperature of 650 °C using rapid thermal annealing (RTA). The preferred orientations of the films were investigated using x-ray diffraction and glancing angle x-ray diffraction. The microstructure and the selected area diffraction pattern of the PZT thin films were also investigated using scanning electron microscopy (SEM) and transmission electron microscopy (TEM), respectively.

Type
Articles
Copyright
Copyright © Materials Research Society 1997

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

1.Kwork, C. K. and Desu, S. B., J. Mater. Res. 8, 339 (1993).Google Scholar
2.Yoon, D. S., Kim, J. M., Ann, K. C., and No, K., Integrated Ferroelectrics 4, 93 (1994).CrossRefGoogle Scholar
3.Tani, T., Xu, Z., and Payne, D. A., in Ferroelectric Thin Films III, edited by Tuttle, B. A., Myers, E. R., Desu, S. B., and Lansen, P. K. (Mater. Res. Soc. Symp. Proc. 310, Pittsburgh, PA, 1993), p. 269.Google Scholar
4.Kim, C. J., Yoon, D. S., Lee, J. S., Choi, C. G., and No, K., Jpn. Appl. Phys. 33, 2675 (1994).CrossRefGoogle Scholar
5.Krishnakumar, S., Esener, S. C., Fan, C., Ozguz, V. H., Title, M. A., Cozzolino, C., and Lee, S. H., in Ferroelectric Thin Films, edited by Myers, E. R. and Kingon, A. I. (Mater. Res. Soc. Symp. Proc. 200, Pittsburgh, PA, 1990), p. 91.Google Scholar
6.Takahashi, Y. and Yamaguchi, K., J. Mater. Sci. 25, 3950 (1990).CrossRefGoogle Scholar
7.Hsueh, C. C. and Mecartney, M. L., J. Mater. Res. 6, 2208 (1991).CrossRefGoogle Scholar
8.Chapin, L. N. and Myers, S. A., in Ferroelectric Thin Films, edited by Myers, E. R. and Kingon, A. I., Pittsburgh, PA, 1990), p. 153.Google Scholar
9.Yi, G., Wu, Z., and Sayer, M., J. Appl. Phys. 64, 2717 (1988).CrossRefGoogle Scholar
10.Bellur, K. R., Al-Shareet, H. N., Rou, S. H., Gifford, K. D., Auciello, O., and Kingon, A. I., ISAF Symp. Proc. 8, 448 (1992).Google Scholar
11.Kim, C. J., Yoon, D. S., Lee, J. S., Choi, C. G., Lee, W. J., and No, K., J. Appl. Phys. 76 (11), 7478 (1994).CrossRefGoogle Scholar
12.Takayama, R. and Tomita, Y., J. Appl. Phys. 65, 1666 (1989).CrossRefGoogle Scholar
13.Brooks, K. G., Reaney, I. M., Klissurska, R., Huang, Y., Bursill, L., and Setter, N., J. Mater. Res. 9, 2540 (1994).CrossRefGoogle Scholar
14.Budd, K. D., Dey, S. K., and Payne, D. A., in Better Ceramics Through Chemistry II, edited by Brinker, C. J., Clark, D. E., and Ulrich, D. R. (Mater. Res. Soc. Symp. Proc. 73, Pittsburgh, PA, 1986), p. 711.Google Scholar
15.Lakeman, C. D. E., Campion, J-F., and Payne, D. A., in Ceramic Transactions 25, edited by A. S. Bhalla and K. M. Nair (1992), p. 413.Google Scholar