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High catalytic performance of Fe-rich palygorskite clay-supported Ni catalysts for steam reforming of toluene

Published online by Cambridge University Press:  11 May 2023

Minghao Ji ,
Xuehua Zou ,
Haibo Liu ,
Yinsheng Zhang ,
Shiwei Dong ,
Chengrui Xu ,
Qiaoqin Xie ,
Dong Chen ,
Chengzhu Zhu  and
Tianhu Chen
Minghao Ji
Affiliation:
Institute of Environmental Minerals and Materials, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China Key Laboratory of Nano-minerals and Pollution Control of Anhui Higher Education Institutes, Hefei University of Technology, Hefei 230009, China Institute of Atmospheric Environment & Pollution Control Engineering, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China
Xuehua Zou*
Affiliation:
Institute of Environmental Minerals and Materials, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China Key Laboratory of Nano-minerals and Pollution Control of Anhui Higher Education Institutes, Hefei University of Technology, Hefei 230009, China Institute of Atmospheric Environment & Pollution Control Engineering, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China
Haibo Liu
Affiliation:
Institute of Environmental Minerals and Materials, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China Key Laboratory of Nano-minerals and Pollution Control of Anhui Higher Education Institutes, Hefei University of Technology, Hefei 230009, China Institute of Atmospheric Environment & Pollution Control Engineering, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China
Yinsheng Zhang
Affiliation:
Institute of Environmental Minerals and Materials, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China Key Laboratory of Nano-minerals and Pollution Control of Anhui Higher Education Institutes, Hefei University of Technology, Hefei 230009, China Institute of Atmospheric Environment & Pollution Control Engineering, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China
Shiwei Dong
Affiliation:
Institute of Environmental Minerals and Materials, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China Key Laboratory of Nano-minerals and Pollution Control of Anhui Higher Education Institutes, Hefei University of Technology, Hefei 230009, China Institute of Atmospheric Environment & Pollution Control Engineering, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China
Chengrui Xu
Affiliation:
Institute of Environmental Minerals and Materials, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China Key Laboratory of Nano-minerals and Pollution Control of Anhui Higher Education Institutes, Hefei University of Technology, Hefei 230009, China Institute of Atmospheric Environment & Pollution Control Engineering, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China
Qiaoqin Xie
Affiliation:
Institute of Environmental Minerals and Materials, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China Key Laboratory of Nano-minerals and Pollution Control of Anhui Higher Education Institutes, Hefei University of Technology, Hefei 230009, China Institute of Atmospheric Environment & Pollution Control Engineering, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China
Dong Chen
Affiliation:
Institute of Environmental Minerals and Materials, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China Key Laboratory of Nano-minerals and Pollution Control of Anhui Higher Education Institutes, Hefei University of Technology, Hefei 230009, China Institute of Atmospheric Environment & Pollution Control Engineering, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China
Chengzhu Zhu
Affiliation:
Institute of Environmental Minerals and Materials, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China Key Laboratory of Nano-minerals and Pollution Control of Anhui Higher Education Institutes, Hefei University of Technology, Hefei 230009, China Institute of Atmospheric Environment & Pollution Control Engineering, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China
Tianhu Chen*
Affiliation:
Institute of Environmental Minerals and Materials, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China Key Laboratory of Nano-minerals and Pollution Control of Anhui Higher Education Institutes, Hefei University of Technology, Hefei 230009, China Institute of Atmospheric Environment & Pollution Control Engineering, School of Resources and Environmental Engineering, Hefei University of Technology, Hefei 230009, China
*
*Email: chentianhu@hfut.edu.cn
*Email: chentianhu@hfut.edu.cn
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Abstract

The development and application of Fe-rich palygorskite clay has been restricted significantly by its red colour and low grade. Moreover, the nano-structured properties of palygorskite and the relatively large Fe content of Fe-rich palygorskite clay have received insufficient attention. The present study involved the synthesis of Ni-based catalysts via a coprecipitation method using Fe-rich palygorskite clay as the support. The catalysts were then evaluated for their performance for catalytic steam reforming of toluene (CSRT). The experimental findings revealed that the Fe in Fe-rich palygorskite clay interacted strongly with Ni and formed Fe-Ni alloys. The catalyst with a Ni/Fe mass ratio of 14 (Ni14/FePal) calcined in air at 600°C exhibited superior performance for CSRT under the reaction temperature 700°C and S/C molar ratio of 1.0. According to the kinetics study, Ni14/FePal exhibited the lowest apparent activation energy (33.99 kJ mol−1) among the catalysts, which further confirmed the superior catalytic activity in CSRT. The characterizations of the catalysts used demonstrated that the excellent stability and resistance to coke formation of Ni14/FePal were attributable to the presence of a sufficient amount of highly dispersed Fe-Ni alloys on its surface.

Keywords

Biomass tarFe-Ni alloysFe-rich palygorskite claysteam reformingtoluene
Type
Article
Information
Clay Minerals , Volume 58 , Issue 1 , March 2023 , pp. 67 - 81
Copyright
Copyright © The Author(s), 2023. Published by Cambridge University Press on behalf of The Mineralogical Society of the United Kingdom and Ireland

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Footnotes

Associate Editor: Chun Hui Zhou

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