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Specimen Preparation for X-Ray Fluorescence Analysis of Solutions

Published online by Cambridge University Press:  06 March 2019

L.E. Eksperiandova ,
Z.M. Spolnik  and
A.B. Blank
L.E. Eksperiandova
Affiliation:
Institute for Single Crystals Kharkov, Ukraine
Z.M. Spolnik
Affiliation:
Institute for Single Crystals Kharkov, Ukraine
A.B. Blank
Affiliation:
Institute for Single Crystals Kharkov, Ukraine
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Abstract

Specimens for x-ray fluorescence analysis (XRFA) were prepared by adding dry gelatine (10%) to the analysis solution, homogenizing the mixture and cooling for 20 minutes. Thus, a compact resilient mass could be formed with the required shape and size; the roughness of the surface was determined by the roughness of the surface on which the specimen was formed, much the same as highly polished. Various calibration methods can be applied in the XRFA of a variety of materials if such specimens are used.

Type
IX. XRS Mathematical Methods, Trace Analysis and Other Applications
Information
Advances in X-Ray Analysis , Volume 38: Forty-third Annual Conference on Applications of X-ray Analysis , 1994 , pp. 735 - 739
Copyright
Copyright © International Centre for Diffraction Data 1994

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