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A Low-High Temperature Camera for In-Situ X-Ray Diffraction Studies of Catalysts

Published online by Cambridge University Press:  06 March 2019

J. Pielaszek  and
J.B. Cohen
J. Pielaszek
Affiliation:
Department of Materials Science and Engineering, The Technological Institute, Northwestern University, Evanston Illinois 60201
J.B. Cohen
Affiliation:
Department of Materials Science and Engineering, The Technological Institute, Northwestern University, Evanston Illinois 60201
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Extract

X-Ray diffraction studies of substances under controlled atmospheres and at different temperatures are of great importance in many research areas. This is especially true in the area of catalysis, where the correlation of structural and catalytic properties is needed. The camera described here was made for this purpose although any sample in the powdered form can be studied as well. Many catalysts are in the form of highly dispersed metal deposited on a granulated support. The content of metal may vary from a few tenths to several percent. In a camera used by Janko and Borodzinski a small amount of catalyst was spread out on a porous silica glass sample holder which then was placed in a high temperature XRD camera with flowing gas of controlled composition.

Type
III. Position Sensitive Detectors and X-Ray Instrumentation
Information
Advances in X-Ray Analysis , Volume 27: Thirty-Second Annual Conference on Applications of X-ray Analysis, August 1-5, 1983 , 1983 , pp. 285 - 291
Copyright
Copyright © International Centre for Diffraction Data 1983

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References

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