Hostname: page-component-76fb5796d-vfjqv Total loading time: 0 Render date: 2024-04-26T11:12:55.264Z Has data issue: false hasContentIssue false

Bulge test and AFM point deflection method, two technics for the mechanical characterisation of very low stiffness freestanding films

Published online by Cambridge University Press:  14 January 2009

P. Martins
Affiliation:
Université de Lyon, INSA-Lyon, INL, CNRS UMR 5270, 69621 Villeurbanne, France
P. Delobelle*
Affiliation:
FEMTO-ST, LMARC, CNRS UMR 6174, 25000 Besançon, France
C. Malhaire
Affiliation:
Université de Lyon, INSA-Lyon, INL, CNRS UMR 5270, 69621 Villeurbanne, France
S. Brida
Affiliation:
AUXITROL SA, Esterline Sensors Group, 18941 Bourges Cedex 9, France
D. Barbier
Affiliation:
Université de Lyon, INSA-Lyon, INL, CNRS UMR 5270, 69621 Villeurbanne, France
Get access

Abstract

The aim of this work is to compare several methods for the determination of very thin films Young's modulus and stress state: the nanoindentation test, the bulge test and the point-deflection method. The tested structures were silicon nitride and silicon nitride/silicon oxide bilayer membranes with different shapes (square or rectangular) and dimensions (from 1 mm to 3 mm). We report new experimental results on submicron thick dielectric membranes with thicknesses down to 100 nm. A Young's modulus of 217 ± 14 GPa have been found for silicon nitride membranes with a residual stress of 411 ± 30 MPa using the bulge test. Using nanoindentation experiments, a Young's modulus higher than 190 GPa has been estimated. The bulge test is still valid for the studied high dimension to thickness ratio membranes and more appropriate to determine the Young's modulus. A mixture law was shown to be possibly applied for Si3N4/SiO2 bilayer membranes for the Young's modulus and stress determination. The point deflection method is limited by the very low stiffness of these structures and only the residual stress can be accurately extracted. As the Young's modulus and membrane geometry have no significant influence on the stress determination by means of the point deflection method for the studied membranes (with a high lateral dimension to thickness ratio), more reliable results have been obtained such as 487 ± 40 MPa using an AFM cantilever for load-deflection experiments, for Si3N4 thin films.

Keywords

Type
Research Article
Copyright
© EDP Sciences, 2008

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Martins, P., Béclin, S., Brida, S., Metivet, S., Stojanovic, O., Malhaire, C., Microsyst. Technol. 13, 1495 (2007) CrossRef
Y. Zhu, H.D. Espinosa, Reliability of capacitive switches at high and low temperatures (Wiley Periodicals, 2004), p. 317
Lixian, Z., Tongxi, Y., Yapu, Z., Acta Mech. Sinica 20, 178 (2004) CrossRef
Arzt, E., Acta Mater. 46, 5611 (1998) CrossRef
Xiang, X., Chen, X., Vlassak, J.J., Mat. Res. Soc. Symp. Proc. 695, 189 (2002)
Chen, S., Baughn, T.V., Yao, Z.J., Goldsmith, C.L., J. Microelectr. Syst. 11, 309 (2002) CrossRef
Choi, Y., Suresh, S., Acta Mater. 50, 1881 (2002) CrossRef
Florando, J.N., Nix, W.D., J. Mech. Phys. Solids 53, 619 (2005) CrossRef
King, R.B., Int. J. Sol. Struct. 23, 1657 (1987) CrossRef
Ahn, J.-H., Jeon, E.-C., Choi, Y., Lee, Y.-H., Kwon, D., Curr. Appl. Phys. 2, 525 (2002) CrossRef
Saha, R., Nix, W.D., Acta Mater. 50, 23 (2002) CrossRef
Vinci, R.P., Vlassak, J.J., Annu. Rev. Mater. Sci. 26, 431 (1996) CrossRef
Von Preissig, F.J., J. Appl. Phys. 66, 4262 (1989) CrossRef
Kraft, O., Volkert, C.A., Adv. Eng. Mater. 3, 99 (2001) 3.0.CO;2-2>CrossRef
W.N. Sharpe Jr, Mechanical Properties of MEMS Materials, The MEMS Handbook (CRC Press, Boca Raton, FL, 2001), p. 3-1-3-33
Y. Xiang, T.Y. Tsui, J.J. Vlassak, A.J. McKerrow, Measuring the elastic modulus and ultimate strength of low-k dielectric materials by means of the bulge test, in IEEE Int. Interconnect Technol. Conf., San Francisco, CA, USA, 2004
Tripp, M.K., Stampfer, C., Miller, D.C., Helbling, T., Herrmann, C.F., Hierold, C., Gall, K., George, S.M., Bright, V.M., Sens. Actuat. A 130, 419 (2006) CrossRef
Hong, S., Weihs, T.P., Bravman, J.C., Nix, D., J. Electr. Mater. 19, 903 (1990) CrossRef
Poilane, C., Delobelle, P., Lexcellent, C., Hayashi, S., Tobushi, H., Thin Solid Films 379, 156 (2000) CrossRef
Engelstad, R.L., Tang, N., Lovell, E.G., Microelectr. Eng. 61, 271 (2002)
Begleya, M.R., Mackin, T.J., J. Mech. Phys. Solids 52, 2005 (2004) CrossRef
Józwik, M., Delobelle, P., Gorecki, C., Sabac, A., Nieradko, L., Meunier, C., Munnick, F., Thin Solid Films 468, 84 (2004) CrossRef
J. Thévenet, P. Delobelle, P. Blind, V. Petrini, M. De Labachelerie, Étude mécanique de micromiroirs sphériques réalisés par flambage de membranes minces multicouches, 17e Congrès Français de Mécanique-CFM'05, Troyes, Août-Septembre 2005, Paper No. 1264
Zhang, R., Shilo, D., Ravichandran, G., Bhattacharya, K., J. Appl. Mech. 73, 730 (2006) CrossRef
Lesemana, Z.C., Mackin, T.J., Sens. Actuat. 134, 264 (2007) CrossRef
Markutsya, S., Jiang, C., Pikus, Y., Tsukruk, V.V., Adv. Funct. Mater. 15, 771 (2005) CrossRef
B.R. Bracio, R.J. Fasching, F. Kohl, J. Krocza, A smart thin film flow sensors for biomedical applications, in Proc. 22nd Annual EMBS Int. Conf., July 23–28, Chicago, IL, 2000
Guidi, V., Cardinali, G.C., Dori, L., Faglia, G., Ferroni, M., Martinelli, G., Nelli, P., Sberveglieri, G., Sens. Actuat. 49, 88 (1998) CrossRef
Watanabe, H., Vendamme, R., Kunitake, T., Bull. Chem. Soc. Jpn 80, 433 (2007) CrossRef
Olivier, W.C., Pharr, G.M., J. Mater. Res. 7, 1564 (1992) CrossRef
Tabata, O., Kawahata, K., Sugiyama, S., Igarishi, I., Sens. Actuat. 20, 135 (1989) CrossRef
J.Y. Pan, P. Lin, F. Maseeh, S.D. Senturia, Tech. Digest, in IEEE Solid-State Sensor and Actuators Workshop, Hilton Head, SC, Vol. 191 (1990), pp. 70–73
Vlassak, J., Nix, W.D., J. Mater. Res. 7, 3242 (1992) CrossRef
Maier-Schneider, D., Maibach, J., Obermeier, E., J. Microelectromech. Syst. 4, 238 (1995) CrossRef
Bonnotte, E., Delobelle, P., Bornier, L., Trolard, B., Tribillon, G., J. Mater. Res. 12, 2234 (1997) CrossRef
K. Danaie, Membranes micro-usinées par gravure chimique anisotrope: application à la caractérisation des films minces, Thesis, Université Pierre et Marie Curie, Paris VI, 2002
Shojaei, O.R., Karimi, A., Thin Solid Films 332, 202 (1998) CrossRef
Lau, S.T., Chan, H.L.W., Choy, C.L., Cheung, W.Y., Wong, S.P., Integrat. Ferroelect. 69, 375 (2005) CrossRef
Taylor, J.A., J. Vac. Sci. Technol. A 9, 2464 (1991) CrossRef
Kim, M.T., Thin Solid Films 283, 12 (1996) CrossRef
Zhang, T.-Y., Su, Y.-J., Qian, C.-F., Zhao, M.-H., Chen, L.-Q., Acta Mater. 48, 2843 (2000) CrossRef
Edwards, R.L., Coles, G., Sharpe, W.N., Exp. Mech. 44, 49 (2004) CrossRef
Zhang, R., Shilo, D., Ravichandran, G., Bhattacharya, K., J. Appl. Mech. 73, 730 (2006) CrossRef
Zohni, O., Buckner, G., Kim, T., Kingon, A., Maranchi, J., Siergiej, R., J. Micromech. Microeng. 17, 1042 (2007) CrossRef