Hostname: page-component-cd9895bd7-gbm5v Total loading time: 0 Render date: 2024-12-21T14:03:24.594Z Has data issue: false hasContentIssue false

X-ray powder diffraction data for gemcitabine, C9H11F2N3O4

Published online by Cambridge University Press:  20 February 2015

Di Wu
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Pei Xiao Tang
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Shan Shan Li
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Hao Zhong Luo
Affiliation:
Chendu Foreign Languages School, Chengdu 611731, China
Hui Li*
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
*
a)Author to whom correspondence should be addressed. Electronic mail: lihuilab@sina.com

Abstract

X-ray powder diffraction data, unit-cell parameters and space group for gemcitabine, C9H11F2N3O4, are reported [a = 17.641(8) Å, b = 6.985(1) Å, c = 18.653(2) Å, α = β = γ = 90°, unit-cell volume V = 2298.61 Å3, Z = 8 and space group Pmna]. All measured lines were indexed and are consistent with the Pmna space group. No detectable impurities were observed.

Type
New Diffraction Data
Copyright
Copyright © International Centre for Diffraction Data 2015 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Engel, G. E., Wilke, S., König, O., Harris, K. D. M., and Leusen, F. J. J. (1999). “Powder Solve–a complete package for crystal structure solution from powder diffraction patterns,” J. Appl. Crystalogr. 32, 11691179.Google Scholar
Li, S. S., Wu, X. Q., Pan, Q. Q., Cheng, Q., and Li, H. (2014). “Comparison of the accuracy of powder and single crystal X-ray diffraction techniques in determining organic crystal structure,” Chin. Sci. Bull. 59, 497501.Google Scholar
Mini, E., Nobili, S., Caciagli, B., Landini, I., and Mazzei, T. (2006). “Cellular pharmacology of gemcitabine,” Ann. Oncol. 17, v7v12.Google Scholar
Moysan, E., Bastiat, G., and Benoit, J. P. (2013). “Gemcitabine versus modified gemcitabine: a review of several promising chemical Modifications,” Mol. Pharm. 10, 430444.Google Scholar
Pan, Q. Q., Guo, P., Duan, J., Cheng, Q., and Li, H. (2012). “Comparative crystal structure determination of griseofulvin: powder X-ray diffraction versus Single-crystal X-ray diffraction,” Chin. Sci. Bull. 57, 38673871.CrossRefGoogle Scholar
Plunkett, W., Huang, P., and Gandhi, V. (1995). “Preclinical characteristics of gemcitabine,” Anti-cancer Drugs 6, 713.CrossRefGoogle ScholarPubMed
Wu, D., Li, S. S., Xu, K. L., Zhang, L. L., Wu, X. Q., and Li, H. (2014). “X-ray powder diffraction data for loratadine,” Powder Diffr. 29(2), 193195.CrossRefGoogle Scholar
Young, R. A. (1993). The Rietveld Method, IUCr Monographies of Crystallography (Wiley, Oxford).Google Scholar
Supplementary material: File

Wu supplementary material

Wu supplementary material 1

Download Wu supplementary material(File)
File 113.9 KB