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Structural Characterization of Iron Nanoparticles Synthesized by Chemical -Methods

Published online by Cambridge University Press:  31 January 2012

A. Ruíz-Baltazar ,
Claudia López ,
R. Pérez  and
G. Rosas
A. Ruíz-Baltazar
Affiliation:
Instituto de Investigaciones Metalúrgicas, UMSNH, Edificio U, Ciudad Universitaria, CP 58060, Morelia Michoacán, MEXICO. Email: alvarodejesusruiz@yahoo.com.mx
Claudia López
Affiliation:
Instituto de Investigaciones Metalúrgicas, UMSNH, Edificio U, Ciudad Universitaria, CP 58060, Morelia Michoacán, MEXICO. Email: alvarodejesusruiz@yahoo.com.mx
R. Pérez
Affiliation:
Centro de Física Aplicada y Tecnología Avanzada, Boulevard Juriquilla 3001, Juriquilla Querétaro, MEXICO CP 76230.
G. Rosas
Affiliation:
Instituto de Investigaciones Metalúrgicas, UMSNH, Edificio U, Ciudad Universitaria, CP 58060, Morelia Michoacán, MEXICO. Email: alvarodejesusruiz@yahoo.com.mx
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Abstract

Different synthesis methods has been employed to produce nanoparticles, however, chemical reduction method offer a effective route to obtained sizes nanoparticles controlled and morphologies very well defined. Iron nanoparticles were synthesized by chemical reduction using sodium borohydride (SB) NaBH4, Fe (III) Chloride hexahydrate (FeCl3·6H2O) as starting metallic salt (MS) and Poly-vinyl pyrrolidone (PVP) as surfactant agent. The nanoparticles have been characterized by transmission electron microscopy (TEM) and UV-Vis spectroscopy.

Keywords

Fechemical synthesistransmission electron microscopy (TEM)nanoscalenanostructure
Type
Articles
Information
MRS Online Proceedings Library (OPL) , Volume 1372: Symposium S3 – Structural and Chemical Characterization of Metal Alloys and Compounds—2011 , 2012 , imrc-1372-s3-p27
Copyright
Copyright © Materials Research Society 2012

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References

REFERENCES

1. Guo, L., Huang, Q., Li, X. and Yang, S., Phys. Chem. Chem. Phys. 3, 1661–1665 (2001).Google Scholar
2. Volokitin, Y., Sinzig, J., de Jong, L., Schmid, G., Vargaftic, M. N. and Moiseev, I. I., Nature 384, 621 (1998).Google Scholar
3. Sun, S., Murray, C.B., Weller, D., Folks, L., Moser, A., Science 287, 1989–1992 (2000).Google Scholar
4. Sun, Y.P., Li, X.Q., Zhang, W.X., Wang, H., Physicochem. Eng. Aspects 308, 60–66 (2007).Google Scholar
5. Li, L., Fan, M., Brown, R.C., Van Leeuwen, J., Wang, J., Wang, W., Song, Y., Zhang, P., Critical Reviews in Environmental Science and Technology 36, 405–431 (2006).Google Scholar
6. Kim, T.S., Sun, W., Choi, C.J., Lee, B.T., Rev. Adv Mater Sci. 5, 481–486 (2003).Google Scholar
7. Zhao, L.Y., Eldridge, KR., Sukhija, K, Jalili, H., Heinig, N.F., Luenga, K.T., Appl. Phys. Letters 88, 11–33 (2006).Google Scholar
8. Hoder, T., Kudrle, V., Frgala, Z, Janca, J. WDS’05 Proceedings of Contributed Papers II, 300–305 (2005).Google Scholar
9. Li, X.Q., Elliott, D.W., and Zhang, W.X., Materials and Engineering Aspects . Critical Reviews in Solid State and Materials Sciences, 31, 111–122 (2006).Google Scholar
10. Wilcoxon, J.P., Martin, J.E., Provencio, P., Langmuir 16, 9912 (2000).Google Scholar
11. Sun, Y.P., Li, X.Q, Cao, J., Zhang, W. X., Wang, H. P., Advances in Colloid and Interface Science 120, 47–56 (2006).Google Scholar
12. Diao, M., Yao, M., Water Research 43, 5243 – 5251 (2009).Google Scholar
13. Lee, H.Y, Lee, S.H, Xu, C., Xie, J., Lee, J.H., Wu, B., Koh, A. L., Wang, X., Sinclair, R., Wang, S., Nishimura, D. G, Biswal, S., Sun, S., Cho, S. H. and Chen, X., Nanotechnology 19, 165101 (2008).Google Scholar
14. Lung, H., Welliot, D., Pang, Y., Journal of Environmental Engineering and Management 16, 371–380 (2006).Google Scholar
15. Sinnott, S.B., Andrews, R., Qian, D., Rao, A.M., Mao, Z., Dickey, E.C., Derbyshire, F., Chem. Phys. Letters 315, 25–30 (1999).Google Scholar
16. Guo, Z., Henry, L., and Podlaha, E.J., ECS Transactions 1 (12), 63-69 (2006).Google Scholar