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The Microstructures and Grain Boundary Segregations of Ceramic Barium Titanate Processed in Microwave Field

Published online by Cambridge University Press:  01 February 2011

Hanxing Liu
Affiliation:
State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Luoshi Road 122, Wuhan 430070, P.R. China
Zhongqin Tian
Affiliation:
State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Luoshi Road 122, Wuhan 430070, P.R. China
Jian Zhou
Affiliation:
State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Luoshi Road 122, Wuhan 430070, P.R. China
Hongtao Yu
Affiliation:
State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Luoshi Road 122, Wuhan 430070, P.R. China
Long Zou
Affiliation:
State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Luoshi Road 122, Wuhan 430070, P.R. China
Shixi Ouyang
Affiliation:
State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Luoshi Road 122, Wuhan 430070, P.R. China
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Abstract

Ceramic sintering in microwave field is a new ceramic processing method. In present paper, we detected the microstructures and boundary segregation of BaTiO3 ceramics which were sintered in microwave field. Scanning electron microscopy(SEM), and transmission electron microscopy(TEM), and chemical analysis methods were employed to detect the microstructure of BaTiO3, element distribution near the boundary of BaTiO3 ceramic. The results shown growth of grain of the ceramic was influenced by impurities such as acceptor, benefactor et al, and the element distribution near the grain boundary of BaTiO3 sintered in microwave field were different with that sintered in conventional method. The boundary segregations of BaTiO3 sintered in microwave field were not obvious as compared to the conventional method because the diffusion was enhanced due to the microwave field.

Type
Research Article
Copyright
Copyright © Materials Research Society 2004

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