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Magnetic Properties and Fabrication of Monodisperse FePd Nanoparticles

Published online by Cambridge University Press:  21 March 2011

Yanglong Hou
Affiliation:
Department of Chemistry, School of Science, The University of Tokyo, Tokyo 113-0033, Japan
Hiroshi Kondoh
Affiliation:
Department of Chemistry, School of Science, The University of Tokyo, Tokyo 113-0033, Japan
Toshiaki Ohta
Affiliation:
Department of Chemistry, School of Science, The University of Tokyo, Tokyo 113-0033, Japan, Fax: 81-3-38121896; Tel:81-3-58414333; E-mail: ohta@chem.s.u-tokyo.ac.jp
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Abstract

The combination of 1-adamantanecarboxylic acid and tri-alkylphosphine was applied to produce monodisperse FePd nanoparticles by the polyol reduction of palladium acetylacetonate and thermally decomposition of iron pentacarbonyl. Images of high resolution transmission electron microscopy (TEM) and X-ray diffraction (XRD) data indicate a highly monodisperse and crystalline nature of the FePd nanoparticles. Magnetic studies performed by Quantum Design SQUID magnetometer show that FePd (16nm) nanoparticles are superparamagnetic at room temperature.

Type
Research Article
Copyright
Copyright © Materials Research Society 2004

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